N,N-bis(4-methoxybenzyl)-4-[1-(4-fluorophenyl)-3-trifluoromethyl-1H-pyrazol-5-yl]benzenesulfonamide

Base Information

• Chemical Name: N,N-bis(4-methoxybenzyl)-4-[1-(4-fluorophenyl)-3-trifluoromethyl-1H-pyrazol-5-yl]benzenesulfonamide
• CAS No.: 170570-96-4
• Molecular Formula: C₃₂H₂₇F₄N₃O₄S
• Molecular Weight: 625.644

Synonyms:N,N-bis(4-methoxybenzyl)-4-[1-(4-fluorophenyl)-3-trifluoromethyl-1H-pyrazol-5-yl]benzenesulfonamide

Chemical Property of N,N-bis(4-methoxybenzyl)-4-[1-(4-fluorophenyl)-3-trifluoromethyl-1H-pyrazol-5-yl]benzenesulfonamide

Chemical Property:

Purity/Quality:

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Technology Process of N,N-bis(4-methoxybenzyl)-4-[1-(4-fluorophenyl)-3-trifluoromethyl-1H-pyrazol-5-yl]benzenesulfonamide

There total 4 articles about N,N-bis(4-methoxybenzyl)-4-[1-(4-fluorophenyl)-3-trifluoromethyl-1H-pyrazol-5-yl]benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

→ N,N-bis(4-methoxybenzyl)-4-[1-(4-fluorophenyl)-3-trifluoromethyl-1H-pyrazol-5-yl]benzenesulfonamide (170570-96-4)

Guidance literature:

Reference yield:

4-acetylbenzenesulfonamide (1565-17-9) → N,N-bis(4-methoxybenzyl)-4-[1-(4-fluorophenyl)-3-trifluoromethyl-1H-pyrazol-5-yl]benzenesulfonamide (170570-96-4)

Guidance literature:

Multi-step reaction with 3 steps

1: 1.) NaH, DMSO / 1.) 45 min, 2.) RT, 24 h

2: NaOMe / methanol / 24 h / Heating

3: ethanol / 20 h / Heating

With sodium methylate; sodium hydride; dimethyl sulfoxide; In methanol; ethanol;

DOI:10.1021/jm960803q

Reference yield:

p-Methoxybenzyl bromide (2746-25-0) → N,N-bis(4-methoxybenzyl)-4-[1-(4-fluorophenyl)-3-trifluoromethyl-1H-pyrazol-5-yl]benzenesulfonamide (170570-96-4)

Guidance literature:

Multi-step reaction with 3 steps

1: 1.) NaH, DMSO / 1.) 45 min, 2.) RT, 24 h

2: NaOMe / methanol / 24 h / Heating

3: ethanol / 20 h / Heating

With sodium methylate; sodium hydride; dimethyl sulfoxide; In methanol; ethanol;

DOI:10.1021/jm960803q

upstream raw materials:

4-acetylbenzenesulfonamide

p-Methoxybenzyl bromide

4-Acetyl-N,N-bis-(4-methoxy-benzyl)-benzenesulfonamide

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