1-[(4-(2-methoxyphenyl)piperazin-1-yl)methyl]-1,2-dicarba-closo-dodecaborane

Base Information

Chemical Name:1-[(4-(2-methoxyphenyl)piperazin-1-yl)methyl]-1,2-dicarba-closo-dodecaborane
CAS No.:1299472-30-2
Molecular Formula:C₁₄H₂₈B₁₀N₂O
Molecular Weight:348.499
Hs Code.:

Synonyms:1-[(4-(2-methoxyphenyl)piperazin-1-yl)methyl]-1,2-dicarba-closo-dodecaborane

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Chemical Property of 1-[(4-(2-methoxyphenyl)piperazin-1-yl)methyl]-1,2-dicarba-closo-dodecaborane

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Technology Process of 1-[(4-(2-methoxyphenyl)piperazin-1-yl)methyl]-1,2-dicarba-closo-dodecaborane

There total 2 articles about 1-[(4-(2-methoxyphenyl)piperazin-1-yl)methyl]-1,2-dicarba-closo-dodecaborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 21057-44-3
1-(2-methoxyphenyl)-4-(prop-2-yn-1-yl)piperazine

: C₄H₁₈B₁₀N₂

: 1299472-30-2
1-[(4-(2-methoxyphenyl)piperazin-1-yl)methyl]-1,2-dicarba-closo-dodecaborane

Guidance literature:: With silver nitrate; In toluene; at 100 ℃; for 16h; Reagent/catalyst; Time; Inert atmosphere; Microwave irradiation;
DOI:10.1021/ic400928v

Reference yield: 27.0%

: 35386-24-4
1-(2-Methoxyphenyl)piperazine

: 19496-84-5
1-bromomethyl-1,2-dicarba-closo-dodecaborane⁽¹²⁾

: 1299472-30-2
1-[(4-(2-methoxyphenyl)piperazin-1-yl)methyl]-1,2-dicarba-closo-dodecaborane

Guidance literature:: With diisopropylethylamine; In tetrahydrofuran; under inert atmosphere; diisopropylethylamine (5.7 mmol) added to stirring soln. of B10H10CHCCH2Br (4.2 mmol) and HNC4H8NC6H4OCH3 (5.2 mmol), heated at reflux for 24 h; filtered upon cooling, solvent removed in vac., chromd. (silica gel, 75-100% CH2Cl2/hexanes), solvent evapd.;
DOI:10.1016/j.ica.2012.03.017

Reference yield:

: 1299472-30-2
1-[(4-(2-methoxyphenyl)piperazin-1-yl)methyl]-1,2-dicarba-closo-dodecaborane

: B₉H₁₀CHCCH₂NC₄H₈NC₆H₄OCH₃^(1-)

Guidance literature:: With NaF; In not given; under inert atmosphere; react. of B complex with NaF under reflux;
DOI:10.1016/j.ica.2012.03.017