4-<<<(2-methylphenyl)amino>carbonyl>amino>phenylacetate N-hydroxysuccinimide ester

Base Information

• Chemical Name: 4-<<<(2-methylphenyl)amino>carbonyl>amino>phenylacetate N-hydroxysuccinimide ester
• CAS No.: 224577-14-4
• Molecular Formula: C₂₀H₁₉N₃O₅
• Molecular Weight: 381.388

Synonyms:4-<<<(2-methylphenyl)amino>carbonyl>amino>phenylacetate N-hydroxysuccinimide ester

Chemical Property of 4-<<<(2-methylphenyl)amino>carbonyl>amino>phenylacetate N-hydroxysuccinimide ester

Chemical Property:

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Technology Process of 4-<<<(2-methylphenyl)amino>carbonyl>amino>phenylacetate N-hydroxysuccinimide ester

There total 5 articles about 4-<<<(2-methylphenyl)amino>carbonyl>amino>phenylacetate N-hydroxysuccinimide ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-aminophenylacetic acid (1197-55-3) → 4-<<<(2-methylphenyl)amino>carbonyl>amino>phenylacetate N-hydroxysuccinimide ester (224577-14-4)

Guidance literature:

Multi-step reaction with 3 steps

1: 75 percent / dimethylformamide / 1 h

2: SOCl₂ / acetonitrile / 0.17 h

3: Et₃N / acetonitrile / 2 h

With thionyl chloride; triethylamine; In N,N-dimethyl-formamide; acetonitrile;

DOI:10.1021/jm980673g

Reference yield:

2-tolyl isocyanate (614-68-6) → 4-<<<(2-methylphenyl)amino>carbonyl>amino>phenylacetate N-hydroxysuccinimide ester (224577-14-4)

Guidance literature:

Multi-step reaction with 3 steps

1: 75 percent / dimethylformamide / 1 h

2: SOCl₂ / acetonitrile / 0.17 h

3: Et₃N / acetonitrile / 2 h

With thionyl chloride; triethylamine; In N,N-dimethyl-formamide; acetonitrile;

DOI:10.1021/jm980673g

Reference yield:

2-{4-[(2-toluidinocarbonyl)amino]phenyl}acetic acid (181517-99-7) → 4-<<<(2-methylphenyl)amino>carbonyl>amino>phenylacetate N-hydroxysuccinimide ester (224577-14-4)

Guidance literature:

Multi-step reaction with 2 steps

1: SOCl₂ / acetonitrile / 0.17 h

2: Et₃N / acetonitrile / 2 h

With thionyl chloride; triethylamine; In acetonitrile;

DOI:10.1021/jm980673g

upstream raw materials:

1-hydroxy-pyrrolidine-2,5-dione

4-aminophenylacetic acid

2-tolyl isocyanate

2-{4-[(2-toluidinocarbonyl)amino]phenyl}acetic acid

Downstream raw materials:

2-{4-[(2-toluidinocarbonyl)amino]phenyl}acetyl-L-leucine

N_α-<<4-<<<(2-methylphenyl)amino>carbonyl>amino>phenyl>acetyl>-N_ε-<6-hexanoyl>-L-lysinyl-L-(α-O-benzylaspartyl)-L-valyl-L-proline benzyl ester

N-<<4-<<<(2-methylphenyl)amino>carbonyl>amino>phenyl>acetyl>-L-leucyl-L-(α-O-benzylaspartyl)-L-O-benzylvaline

dibenzyl N-<<4-<<<(2-methylphenyl)amino>carbonyl>amino>phenyl>acetyl>-L-leucyl-L-α-aspartate

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