C₅₀H₉₆O₈Si₃

Base Information

Chemical Name:C₅₀H₉₆O₈Si₃
CAS No.:945908-23-6
Molecular Formula:C₅₀H₉₆O₈Si₃
Molecular Weight:909.564
Hs Code.:

C<sub>50</sub>H<sub>96</sub>O<sub>8</sub>Si<sub>3</sub>

Synonyms:C₅₀H₉₆O₈Si₃

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Chemical Property of C₅₀H₉₆O₈Si₃

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Technology Process of C₅₀H₉₆O₈Si₃

There total 8 articles about C₅₀H₉₆O₈Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 945908-19-0
C₁₄H₂₉OSiI

: 717916-62-6
(2-{(2R,3S,4S,5S,6R)-4-(tert-Butyl-dimethyl-silanyloxy)-6-[(S)-4-(tert-butyl-dimethyl-silanyloxy)-3-methyl-butyl]-3,5-dimethyl-tetrahydro-pyran-2-yl}-3,4,6-trimethoxy-5-methyl-phenyl)-acetaldehyde

: 945908-23-6
C₅₀H₉₆O₈Si₃

Guidance literature:: With chromium dichloride; nickel dichloride; In N,N-dimethyl-formamide; at 60 ℃; for 3h;
DOI:10.1246/cl.2007.726

Reference yield:

: 945908-20-3
C₁₉H₃₄O₂Si

: 945908-23-6
C₅₀H₉₆O₈Si₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: H₂ / Pd(OH)2/C / dioxane / 3 h / 20 °C

2.1: PDC / CH₂Cl₂ / 3 h / 20 °C

3.1: PPh₃; Et₃N / CH₂Cl₂ / 0.17 h / -78 °C

4.1: 97 percent / n-BuLi / tetrahydrofuran / 2.5 h / -20 - 0 °C

5.1: Cp₂ZrHCl / tetrahydrofuran / 24 h / 20 °C

5.2: 71 percent / I₂ / tetrahydrofuran / 0.5 h / 20 °C

6.1: 90 percent / CrCl₂ / NiCl₂ / dimethylformamide / 3 h / 60 °C

With chromium dichloride; dipyridinium dichromate; Schwartz's reagent; n-butyllithium; hydrogen; triethylamine; triphenylphosphine; palladium dihydroxide; nickel dichloride; In tetrahydrofuran; 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide; 4.1: Corey-Fuchs / 6.1: Noyaki-Hiyama-Kishi coupling;
DOI:10.1246/cl.2007.726

Reference yield:

: C₁₃H₂₀O₂

: 945908-23-6
C₅₀H₉₆O₈Si₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: imidazole / dimethylformamide / 1.5 h / 20 °C

2.1: H₂ / Pd(OH)2/C / dioxane / 3 h / 20 °C

3.1: PDC / CH₂Cl₂ / 3 h / 20 °C

4.1: PPh₃; Et₃N / CH₂Cl₂ / 0.17 h / -78 °C

5.1: 97 percent / n-BuLi / tetrahydrofuran / 2.5 h / -20 - 0 °C

6.1: Cp₂ZrHCl / tetrahydrofuran / 24 h / 20 °C

6.2: 71 percent / I₂ / tetrahydrofuran / 0.5 h / 20 °C

7.1: 90 percent / CrCl₂ / NiCl₂ / dimethylformamide / 3 h / 60 °C

With 1H-imidazole; chromium dichloride; dipyridinium dichromate; Schwartz's reagent; n-butyllithium; hydrogen; triethylamine; triphenylphosphine; palladium dihydroxide; nickel dichloride; In tetrahydrofuran; 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide; 5.1: Corey-Fuchs / 7.1: Noyaki-Hiyama-Kishi coupling;
DOI:10.1246/cl.2007.726