(+/-)9-<(1'-tert-Butyldiphenylsilyloxybut-3'-en-2'-yloxy)methyl>adenine

Base Information

Chemical Name:(+/-)9-<(1'-tert-Butyldiphenylsilyloxybut-3'-en-2'-yloxy)methyl>adenine
CAS No.:136083-15-3
Molecular Formula:C₂₆H₃₁N₅O₂Si
Molecular Weight:473.65
Hs Code.:

Synonyms:(+/-)9-<(1'-tert-Butyldiphenylsilyloxybut-3'-en-2'-yloxy)methyl>adenine

Suppliers and Price of (+/-)9-<(1'-tert-Butyldiphenylsilyloxybut-3'-en-2'-yloxy)methyl>adenine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (+/-)9-<(1'-tert-Butyldiphenylsilyloxybut-3'-en-2'-yloxy)methyl>adenine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (+/-)9-<(1'-tert-Butyldiphenylsilyloxybut-3'-en-2'-yloxy)methyl>adenine

There total 5 articles about (+/-)9-<(1'-tert-Butyldiphenylsilyloxybut-3'-en-2'-yloxy)methyl>adenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 130372-34-8
9-Trimethylsilanyl-9H-purin-6-ylamine

: 136083-14-2
(+/-)-1-tert-Butyldiphenylsilyloxy-2-acetoxymethylenoxybut-3-ene

: 136083-15-3
(+/-)9-<(1'-tert-Butyldiphenylsilyloxybut-3'-en-2'-yloxy)methyl>adenine

Guidance literature:: With dibenzo-18-crown-6; potassium iodide; In toluene; acetonitrile; at 80 ℃; for 8h; solid-liquid phase transfer catalysis;

Reference yield:

: 177032-63-2
(+/-)-1-(tert-butyldiphenylsilyloxy)-2-hydroxy-3-butene

: 136083-15-3
(+/-)9-<(1'-tert-Butyldiphenylsilyloxybut-3'-en-2'-yloxy)methyl>adenine

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / P₂O₅ / CHCl₃ / 24 h / Ambient temperature

2: 95 percent / BF₃*Et₂O / diethyl ether / 48 h / 4 °C

3: 65 percent / dibenzo-18-crown-6 ether, KI / acetonitrile; toluene / 8 h / 80 °C / solid-liquid phase transfer catalysis

With dibenzo-18-crown-6; boron trifluoride diethyl etherate; phosphorus pentoxide; potassium iodide; In diethyl ether; chloroform; toluene; acetonitrile;

Reference yield:

: 136083-13-1
(+/-)-1-tert-Butyldiphenylsilyloxy-2-methoxymethylenoxybut-3-ene

: 136083-15-3
(+/-)9-<(1'-tert-Butyldiphenylsilyloxybut-3'-en-2'-yloxy)methyl>adenine

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / BF₃*Et₂O / diethyl ether / 48 h / 4 °C

2: 65 percent / dibenzo-18-crown-6 ether, KI / acetonitrile; toluene / 8 h / 80 °C / solid-liquid phase transfer catalysis

With dibenzo-18-crown-6; boron trifluoride diethyl etherate; potassium iodide; In diethyl ether; toluene; acetonitrile;