C₃₂H₆₀O₅Si₂

Base Information

Chemical Name:C₃₂H₆₀O₅Si₂
CAS No.:952492-24-9
Molecular Formula:C₃₂H₆₀O₅Si₂
Molecular Weight:580.996
Hs Code.:

C<sub>32</sub>H<sub>60</sub>O<sub>5</sub>Si<sub>2</sub>

Synonyms:C₃₂H₆₀O₅Si₂

Suppliers and Price of C₃₂H₆₀O₅Si₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₂H₆₀O₅Si₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₂H₆₀O₅Si₂

There total 12 articles about C₃₂H₆₀O₅Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 952492-23-8
C₃₂H₆₂O₆Si₂

: 952492-24-9
C₃₂H₆₀O₅Si₂

Guidance literature:: C₃₂H₆₂O₆Si₂; With dmap; methanesulfonyl chloride; triethylamine; In dichloromethane; at 0 ℃; for 0.25h;

With potassium carbonate; In methanol; at 20 ℃; for 18h; Further stages.;
DOI:10.1016/j.tetlet.2007.07.068

Reference yield:

: 952492-20-5
C₂₆H₄₄O₄Si

: 952492-24-9
C₃₂H₆₀O₅Si₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: 91 percent / OsO₄; NMO / acetone; H₂O / 72 h / 20 °C

2.1: 2,6-lutidine / CH₂Cl₂ / 0.08 h / 0 °C

3.1: DIBAL-H / CH₂Cl₂ / 0.33 h / -78 °C

4.1: MsCl; Et₃N; DMAP / CH₂Cl₂ / 0.25 h / 0 °C

4.2: 52 percent / K₂CO₃ / methanol / 18 h / 20 °C

With 2,6-dimethylpyridine; dmap; osmium(VIII) oxide; N-methyl-2-indolinone; diisobutylaluminium hydride; methanesulfonyl chloride; triethylamine; In dichloromethane; water; acetone;
DOI:10.1016/j.tetlet.2007.07.068

Reference yield:

: C₃₂H₆₀O₆Si₂

: 952492-24-9
C₃₂H₆₀O₅Si₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: DIBAL-H / CH₂Cl₂ / 0.33 h / -78 °C

2.1: MsCl; Et₃N; DMAP / CH₂Cl₂ / 0.25 h / 0 °C

2.2: 52 percent / K₂CO₃ / methanol / 18 h / 20 °C

With dmap; diisobutylaluminium hydride; methanesulfonyl chloride; triethylamine; In dichloromethane;
DOI:10.1016/j.tetlet.2007.07.068