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(S)-2-((R)-5-Carboxymethyl-4-oxo-2,3,4,5-tetrahydro-benzo[b][1,4]thiazepin-3-ylamino)-4-(tetrahydro-pyran-4-yl)-butyric acid

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  • Chemical Name:(S)-2-((R)-5-Carboxymethyl-4-oxo-2,3,4,5-tetrahydro-benzo[b][1,4]thiazepin-3-ylamino)-4-(tetrahydro-pyran-4-yl)-butyric acid
  • CAS No.:100277-20-1
  • Molecular Formula:C20H26N2O6S
  • Molecular Weight:422.502
  • Hs Code.:
  • Mol file:100277-20-1.mol
(S)-2-((R)-5-Carboxymethyl-4-oxo-2,3,4,5-tetrahydro-benzo[b][1,4]thiazepin-3-ylamino)-4-(tetrahydro-pyran-4-yl)-butyric acid

Synonyms:(S)-2-((R)-5-Carboxymethyl-4-oxo-2,3,4,5-tetrahydro-benzo[b][1,4]thiazepin-3-ylamino)-4-(tetrahydro-pyran-4-yl)-butyric acid

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Chemical Property of (S)-2-((R)-5-Carboxymethyl-4-oxo-2,3,4,5-tetrahydro-benzo[b][1,4]thiazepin-3-ylamino)-4-(tetrahydro-pyran-4-yl)-butyric acid Edit
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Technology Process of (S)-2-((R)-5-Carboxymethyl-4-oxo-2,3,4,5-tetrahydro-benzo[b][1,4]thiazepin-3-ylamino)-4-(tetrahydro-pyran-4-yl)-butyric acid

There total 1 articles about (S)-2-((R)-5-Carboxymethyl-4-oxo-2,3,4,5-tetrahydro-benzo[b][1,4]thiazepin-3-ylamino)-4-(tetrahydro-pyran-4-yl)-butyric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 6 steps
1: benzene / 1 h / Heating
2: H2 / 10 percent Pd-C / ethanol / Ambient temperature
3: 1) NaOEt; 2) H2SO4, LiCl / 1) EtOH, 70 deg C, 60 min; 2) DMSO, 140 deg C, 2.5 h
4: 35 percent / NaBH3CN, molecular sieves 4 Angstroem / acetic acid; ethanol / Ambient temperature
5: 89 percent / 5 N HCl / ethyl acetate / Ambient temperature
6: 98 percent / 1 N NaOH / ethanol / Ambient temperature
With hydrogenchloride; sodium hydroxide; 4 A molecular sieve; sulfuric acid; hydrogen; sodium ethanolate; sodium cyanoborohydride; lithium chloride; palladium on activated charcoal; In ethanol; acetic acid; ethyl acetate; benzene;
DOI:10.1248/cpb.34.1128
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