N,N'-bis(7-hydroxyheptyl)-N,N'-di-p-toluenesulfonyl-1,7-heptanediamine

Base Information

Chemical Name:N,N'-bis(7-hydroxyheptyl)-N,N'-di-p-toluenesulfonyl-1,7-heptanediamine
CAS No.:130945-16-3
Molecular Formula:C₃₅H₅₈N₂O₆S₂
Molecular Weight:666.987
Hs Code.:

Synonyms:N,N'-bis(7-hydroxyheptyl)-N,N'-di-p-toluenesulfonyl-1,7-heptanediamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-bis(7-hydroxyheptyl)-N,N'-di-p-toluenesulfonyl-1,7-heptanediamine

Chemical Property:

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Technology Process of N,N'-bis(7-hydroxyheptyl)-N,N'-di-p-toluenesulfonyl-1,7-heptanediamine

There total 7 articles about N,N'-bis(7-hydroxyheptyl)-N,N'-di-p-toluenesulfonyl-1,7-heptanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 130945-12-9
N,N'-bis<7-(2-tetrahydropyranyloxy)heptyl>-N,N'-di-p-toluenesulfonyl-1,7-heptanediamine

: 130945-16-3
N,N'-bis(7-hydroxyheptyl)-N,N'-di-p-toluenesulfonyl-1,7-heptanediamine

Guidance literature:: With p-toluenesulfonyl chloride; In methanol; for 0.5h; Ambient temperature;

Reference yield:

: 10160-25-5
7-bromo-1-(2-tetrahydropyranyloxy)heptane

: 130945-16-3
N,N'-bis(7-hydroxyheptyl)-N,N'-di-p-toluenesulfonyl-1,7-heptanediamine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DMF, 60 deg C, 20 to 25 mm Hg 2.) DMF, 60 deg C, 3 h

2: 99 percent / p-toluenesulfonyl chloride / methanol / 0.5 h / Ambient temperature

With sodium hydride; p-toluenesulfonyl chloride; In methanol;

Reference yield:

: 10160-24-4
7-bromoheptyl alcohol

: 130945-16-3
N,N'-bis(7-hydroxyheptyl)-N,N'-di-p-toluenesulfonyl-1,7-heptanediamine

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / p-toluenesulfonic acid / diethyl ether / 14 h / Ambient temperature

2: 1.) NaH / 1.) DMF, 60 deg C, 20 to 25 mm Hg 2.) DMF, 60 deg C, 3 h

3: 99 percent / p-toluenesulfonyl chloride / methanol / 0.5 h / Ambient temperature

With sodium hydride; toluene-4-sulfonic acid; p-toluenesulfonyl chloride; In methanol; diethyl ether;