methyl 4,6-O-benzylidene-2,3-dideoxy-2,3-C--α-D-mannopyranoside

Base Information

Chemical Name:methyl 4,6-O-benzylidene-2,3-dideoxy-2,3-C--α-D-mannopyranoside
CAS No.:72079-83-5
Molecular Formula:C₁₉H₂₄O₆
Molecular Weight:348.396
Hs Code.:

methyl 4,6-O-benzylidene-2,3-dideoxy-2,3-C-<R(carboethoxy)ethylidene>-α-D-mannopyranoside

Synonyms:methyl 4,6-O-benzylidene-2,3-dideoxy-2,3-C--α-D-mannopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 4,6-O-benzylidene-2,3-dideoxy-2,3-C--α-D-mannopyranoside

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Technology Process of methyl 4,6-O-benzylidene-2,3-dideoxy-2,3-C--α-D-mannopyranoside

There total 5 articles about methyl 4,6-O-benzylidene-2,3-dideoxy-2,3-C--α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.1%

: 3699-66-9
ethyl 2-diethoxyphosphorylpropionate

: 66537-92-6
methyl 2,3-anhydro-4,6-benzylidene-α-D-allopyranoside

: 72079-83-5
methyl 4,6-O-benzylidene-2,3-dideoxy-2,3-C--α-D-mannopyranoside

Guidance literature:: With sodium hydride; In 1,4-dioxane; at 160 ℃; for 96h;
DOI:10.1016/S0040-4020(01)82414-5

Reference yield: 50.1%

: 29668-62-0
methyl 2-(diethoxyphosphoryl)propanoate

: 66537-92-6
methyl 2,3-anhydro-4,6-benzylidene-α-D-allopyranoside

: 72079-83-5
methyl 4,6-O-benzylidene-2,3-dideoxy-2,3-C--α-D-mannopyranoside

Guidance literature:: With sodium hydride; In 1,4-dioxane; at 160 ℃; for 96h; Mechanism; var. propionates;
DOI:10.1016/S0040-4020(01)82414-5

Reference yield:

: 3699-66-9
ethyl 2-diethoxyphosphorylpropionate

: 66537-92-6
methyl 2,3-anhydro-4,6-benzylidene-α-D-allopyranoside

: 72079-83-5
methyl (2R,4R)-2,3-dideoxy-2,3-<1-(ethoxycarbonyl)ethylidene>-4,6-O-(phenylmethylene)-α-D-mannopyranoside

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1) triglyme, 30 min, room temp., 2) 140 deg C, 4 d;
DOI:10.1021/jo00012a009