Technology Process of C32H42ClN3O7
There total 13 articles about C32H42ClN3O7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium acetate; caesium carbonate;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride;
In
dimethyl sulfoxide;
at 60 ℃;
for 24h;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 5 h / 40 °C
2.1: hydroxylamine hydrochloride / tetrahydrofuran; methanol; water / 0.08 h / 20 °C
3.1: hydrogenchloride; methyl orange; sodium cyanoborohydride / tetrahydrofuran; methanol; water / 3 h / pH 2
4.1: toluene / 14 h / Heating / reflux
5.1: hydrogenchloride / tetrahydrofuran; water / 2 h / 20 °C
6.1: trimethylaluminum / hexanes; dichloromethane / 0.33 h
6.2: 20 °C
6.3: 15 h / 20 °C
7.1: potassium acetate; caesium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 24 h / 60 °C
With
hydrogenchloride; hydroxylamine hydrochloride; methyl orange; trimethylaluminum; potassium acetate; sodium cyanoborohydride; potassium carbonate; caesium carbonate;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride;
In
tetrahydrofuran; methanol; hexanes; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: hydroxylamine hydrochloride / tetrahydrofuran; methanol; water / 0.08 h / 20 °C
2.1: hydrogenchloride; methyl orange; sodium cyanoborohydride / tetrahydrofuran; methanol; water / 3 h / pH 2
3.1: toluene / 14 h / Heating / reflux
4.1: hydrogenchloride / tetrahydrofuran; water / 2 h / 20 °C
5.1: trimethylaluminum / hexanes; dichloromethane / 0.33 h
5.2: 20 °C
5.3: 15 h / 20 °C
6.1: potassium acetate; caesium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 24 h / 60 °C
With
hydrogenchloride; hydroxylamine hydrochloride; methyl orange; trimethylaluminum; potassium acetate; sodium cyanoborohydride; caesium carbonate;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride;
In
tetrahydrofuran; methanol; hexanes; dichloromethane; water; dimethyl sulfoxide; toluene;