Technology Process of C24H30N6O
There total 2 articles about C24H30N6O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
O?(6?chlorobezotriazol?1?yl)?N,N,N,N?tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; 6-chloro-1-hydroxybenzotriazole;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 17.0833h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: N,N-dimethyl acetamide / 15 h / Heating / reflux
2: hydrogenchloride; water / 17 h / 100 °C
3: O?(6?chlorobezotriazol?1?yl)?N,N,N,N?tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; 6-chloro-1-hydroxybenzotriazole / N,N-dimethyl-formamide / 17.08 h / 20 °C
With
hydrogenchloride; O?(6?chlorobezotriazol?1?yl)?N,N,N,N?tetramethyluronium hexafluorophosphate; water; N-ethyl-N,N-diisopropylamine; 6-chloro-1-hydroxybenzotriazole;
In
N,N-dimethyl acetamide; N,N-dimethyl-formamide;
- Guidance literature:
-
C24H30N6O;
With
trichlorophosphate;
In
1,4-dioxane;
at 40 - 80 ℃;
for 3h;
With
sodium carbonate;
In
1,4-dioxane; water;
at 0 ℃;