diethyl 3-((E)-tribenzylstannylmethylene)-4-isopropylcyclopentane-1,1-dicarboxylate

Base Information

Chemical Name:diethyl 3-((E)-tribenzylstannylmethylene)-4-isopropylcyclopentane-1,1-dicarboxylate
CAS No.:1419285-37-2
Molecular Formula:C₃₆H₄₄O₄Sn
Molecular Weight:659.453
Hs Code.:

Synonyms:diethyl 3-((E)-tribenzylstannylmethylene)-4-isopropylcyclopentane-1,1-dicarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl 3-((E)-tribenzylstannylmethylene)-4-isopropylcyclopentane-1,1-dicarboxylate

Chemical Property:

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Technology Process of diethyl 3-((E)-tribenzylstannylmethylene)-4-isopropylcyclopentane-1,1-dicarboxylate

There total 2 articles about diethyl 3-((E)-tribenzylstannylmethylene)-4-isopropylcyclopentane-1,1-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10113-30-1
tribenzyltin hydride

: 133788-02-0
(2-propynyl)-(3-methyl-2-butenyl)propanedioic acid diethyl ester

: 1419285-37-2
diethyl 3-((E)-tribenzylstannylmethylene)-4-isopropylcyclopentane-1,1-dicarboxylate

Guidance literature:: With triethyl borane; In toluene; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.jorganchem.2012.11.007

Reference yield:

: tribenzylchlorostannane

: 1419285-37-2
diethyl 3-((E)-tribenzylstannylmethylene)-4-isopropylcyclopentane-1,1-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / diethyl ether / 0.5 h / 0 °C / Inert atmosphere

2: triethyl borane / toluene / 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; triethyl borane; In diethyl ether; toluene;
DOI:10.1016/j.jorganchem.2012.11.007