2,4,7,9-Tetrachloro-3-hydroxy-8-methoxy-1,6-dimethyl-11H-dibenzo[b,e][1,4]dioxepin-11-one

Base Information

• Chemical Name: 2,4,7,9-Tetrachloro-3-hydroxy-8-methoxy-1,6-dimethyl-11H-dibenzo[b,e][1,4]dioxepin-11-one
• CAS No.: 527-93-5
• Molecular Formula: C16H10Cl4O5
• Molecular Weight: 424.06
• Mol file: 527-93-5.mol

Synonyms:Diploicine;11H-Dibenzo[b,e][1,4]dioxepin-11-one, 2,4,7,9-tetrachloro-3-hydroxy-8-methoxy-1,6-dimethyl-;2,4,7,9-Tetrachloro-3-hydroxy-8-methoxy-1,6-dimethyl-11H-dibenzo[b,E][1,4]dioxepin-11-one;11H-Dibenzo[b,e][1,4]dioxepin-11-one,2,4,7,9-tetrachloro-3-hydroxy-8-methoxy-1,6-dimethyl;Diploicin;

Chemical Property of 2,4,7,9-Tetrachloro-3-hydroxy-8-methoxy-1,6-dimethyl-11H-dibenzo[b,e][1,4]dioxepin-11-one

Chemical Property:

• Vapor Pressure: 1.19E-14mmHg at 25°C
• Melting Point: 233-234°
• Boiling Point: 592.9°C at 760 mmHg
• PKA: 4.87±0.20(Predicted)
• Flash Point: 312.4°C
• PSA: 64.99000
• Density: 1.599g/cm³
• LogP: 5.95610

Purity/Quality:

98%min ^*data from raw suppliers

Diploicin ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: Diploicin is an antibiotic isolated from the lichen Buellia canescens.

Technology Process of 2,4,7,9-Tetrachloro-3-hydroxy-8-methoxy-1,6-dimethyl-11H-dibenzo[b,e][1,4]dioxepin-11-one

There total 1 articles about 2,4,7,9-Tetrachloro-3-hydroxy-8-methoxy-1,6-dimethyl-11H-dibenzo[b,e][1,4]dioxepin-11-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ diploicin (527-93-5)

Guidance literature:

(21);

Reference yield: 93.0%

diploicin (527-93-5) → 3,5-dichloro-6-(3,5-dichloro-2-hydroxy-4-methoxy-6-methylphenoxy)-4-hydroxy-2-methylbenzoate (78135-22-5)

Guidance literature:

With sodium methylate; In methanol;

DOI:10.1039/P19810000849

Reference yield:

diploicin (527-93-5) → 4-hydroxy-6-(2-hydroxy-4-methoxy-6-methylphenoxy)-2-methylbenzoate (69769-51-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 93 percent / sodium methoxide / methanol

2: H₂ / Pd-charcoal

With hydrogen; sodium methylate; palladium on activated charcoal; In methanol;

DOI:10.1039/P19810000849

Downstream raw materials:

3,5-dichloro-6-(3,5-dichloro-2-hydroxy-4-methoxy-6-methylphenoxy)-4-hydroxy-2-methylbenzoate

4-hydroxy-6-(2-hydroxy-4-methoxy-6-methylphenoxy)-2-methylbenzoate

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