C₁₈H₂₂Cl₂N₂O₂

Base Information

Chemical Name:C₁₈H₂₂Cl₂N₂O₂
CAS No.:1333889-95-4
Molecular Formula:C₁₈H₂₂Cl₂N₂O₂
Molecular Weight:369.291
Hs Code.:

C<sub>18</sub>H<sub>22</sub>Cl<sub>2</sub>N<sub>2</sub>O<sub>2</sub>

Synonyms:C₁₈H₂₂Cl₂N₂O₂

Suppliers and Price of C₁₈H₂₂Cl₂N₂O₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₈H₂₂Cl₂N₂O₂

Chemical Property:

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Technology Process of C₁₈H₂₂Cl₂N₂O₂

There total 5 articles about C₁₈H₂₂Cl₂N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2785-78-6
3,6-Dimethylcatechol

: 1333889-95-4
C₁₈H₂₂Cl₂N₂O₂

Guidance literature:: Multi-step reaction with 5 steps

1: potassium hydroxide / dimethyl sulfoxide / Inert atmosphere

2: nitric acid; acetic acid / water / Inert atmosphere

3: palladium 10% on activated carbon; hydrogen / ethanol / Inert atmosphere

4: dichloromethane / Inert atmosphere

5: triethylamine; trichlorophosphate / dichloromethane / 0 °C / Inert atmosphere

With palladium 10% on activated carbon; hydrogen; nitric acid; acetic acid; triethylamine; potassium hydroxide; trichlorophosphate; In ethanol; dichloromethane; water; dimethyl sulfoxide; 1: Williamson synthesis;
DOI:10.1002/pola.24871

Reference yield:

: C₁₈H₂₆Cl₂N₂O₄

: 1333889-95-4
C₁₈H₂₂Cl₂N₂O₂

Guidance literature:: With triethylamine; trichlorophosphate; In dichloromethane; at 0 ℃; Inert atmosphere;
DOI:10.1002/pola.24871

Reference yield:

: 1333889-89-6
C₁₆H₂₂Cl₂N₂O₆

: 1333889-95-4
C₁₈H₂₂Cl₂N₂O₂

Guidance literature:: Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; hydrogen / ethanol / Inert atmosphere

2: dichloromethane / Inert atmosphere

3: triethylamine; trichlorophosphate / dichloromethane / 0 °C / Inert atmosphere

With palladium 10% on activated carbon; hydrogen; triethylamine; trichlorophosphate; In ethanol; dichloromethane;
DOI:10.1002/pola.24871