N-glycyl-N-benzyl>phenylamine

Base Information

Chemical Name:N-glycyl-N-benzyl>phenylamine
CAS No.:106880-77-7
Molecular Formula:C₁₉H₂₄N₂O₄
Molecular Weight:344.411
Hs Code.:

N-glycyl-N-<o-<(2-methoxyethoxy)methoxy>benzyl>phenylamine

Synonyms:N-glycyl-N-benzyl>phenylamine

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Chemical Property of N-glycyl-N-benzyl>phenylamine

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Technology Process of N-glycyl-N-benzyl>phenylamine

There total 4 articles about N-glycyl-N-benzyl>phenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 106880-73-3
benzyl <<benzyl>phenylcarbamoyl>methyl>carbamate

: 106880-77-7
N-glycyl-N-benzyl>phenylamine

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; at 25 ℃; for 1.5h;
DOI:10.1021/ja00240a036

Reference yield:

: 106880-69-7
o-<(2-methoxyethoxy)methoxy>benzaldehyde

: 106880-77-7
N-glycyl-N-benzyl>phenylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / acetic acid, sodium cyanoborohydride / methanol / 36 h / Ambient temperature

2: 1.) NaH / 1.) toluene, 10 min, RT; 2.) 2 min

3: 71 percent / H₂ / 10 percent Pd-C / methanol / 1.5 h / 25 °C

With hydrogen; sodium hydride; sodium cyanoborohydride; acetic acid; palladium on activated charcoal; In methanol;
DOI:10.1021/ja00240a036

Reference yield:

: 90-02-8
salicylaldehyde

: 106880-77-7
N-glycyl-N-benzyl>phenylamine

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) sodium hydride / 1.) THF; 2.) THF, RT, 20 min

2: 96 percent / acetic acid, sodium cyanoborohydride / methanol / 36 h / Ambient temperature

3: 1.) NaH / 1.) toluene, 10 min, RT; 2.) 2 min

4: 71 percent / H₂ / 10 percent Pd-C / methanol / 1.5 h / 25 °C

With hydrogen; sodium hydride; sodium cyanoborohydride; acetic acid; palladium on activated charcoal; In methanol;
DOI:10.1021/ja00240a036