Tetraethylammonium-1,2,3,4-tetrakis(4-methylphenylthio)cyclopentadienid

Base Information

• Chemical Name: Tetraethylammonium-1,2,3,4-tetrakis(4-methylphenylthio)cyclopentadienid
• CAS No.: 131588-70-0
• Molecular Formula: C₈H₂₀N*C₃₃H₂₉S₄
• Molecular Weight: 684.111

Synonyms:Tetraethylammonium-1,2,3,4-tetrakis(4-methylphenylthio)cyclopentadienid

Chemical Property of Tetraethylammonium-1,2,3,4-tetrakis(4-methylphenylthio)cyclopentadienid

Chemical Property:

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Technology Process of Tetraethylammonium-1,2,3,4-tetrakis(4-methylphenylthio)cyclopentadienid

There total 1 articles about Tetraethylammonium-1,2,3,4-tetrakis(4-methylphenylthio)cyclopentadienid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

di(p-tolyl) disulfide (103-19-5) + tetraethylammonium bromide (71-91-0) + cyclopenta-1,3-diene (542-92-7,25568-84-7,7313-32-8) → Tetraethylammonium-1,2,3,4-tetrakis(4-methylphenylthio)cyclopentadienid (131588-70-0)

Guidance literature:

With sodium hydride; Yield given. Multistep reaction; 1a) THF, 0 deg C, b) 4 d, room temperature, 2) CH₂Cl₂;

Reference yield: 95.0%

Tetraethylammonium-1,2,3,4-tetrakis(4-methylphenylthio)cyclopentadienid (131588-70-0) → 1,2,3,4-Tetrakis(4-methylphenylthio)cyclopentadien (131588-56-2)

Guidance literature:

With phosphoric acid; In dichloromethane;

Reference yield: 88.0%

Tetraethylammonium-1,2,3,4-tetrakis(4-methylphenylthio)cyclopentadienid (131588-70-0) → Tetraethylammonium-1,2,3,4-tetrakis(4-methylphenylsulonyl)cyclopentadienid (131588-76-6)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; 1) -15 to -20 deg C, 4 h, 2) 24 h, room temperature;

upstream raw materials:

di(p-tolyl) disulfide

tetraethylammonium bromide

cyclopenta-1,3-diene

Downstream raw materials:

5-(Dimethylaminomethylen)-1,2,3,4-tetrakis(4-methylphenylthio)-1,3-cyclopentadien

1,2,3,4-Tetrakis(4-methylphenylthio)cyclopentadien

1,1'-Bi<3,4,5,5-tetrakis(4-methylphenylthio)-1,3-cyclopentadienyl>

Tetraethylammonium-1,2,3,4-tetrakis(4-methylphenylsulonyl)cyclopentadienid

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