n-[3-(Methylsulfanyl)-9h-fluoren-2-yl]acetamide

Base Information

Chemical Name:n-[3-(Methylsulfanyl)-9h-fluoren-2-yl]acetamide
CAS No.:6098-47-1
Molecular Formula:C16H15NOS
Molecular Weight:269.3614
Hs Code.:
NSC Number:109639
DSSTox Substance ID:DTXSID80296505
Wikidata:Q82037138

Synonyms:n-[3-(methylsulfanyl)-9h-fluoren-2-yl]acetamide;6098-47-1;NSC109639;DTXSID80296505;NSC-109639

Suppliers and Price of n-[3-(Methylsulfanyl)-9h-fluoren-2-yl]acetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of n-[3-(Methylsulfanyl)-9h-fluoren-2-yl]acetamide

Chemical Property:

Vapor Pressure:1.52E-09mmHg at 25°C
Boiling Point:484.6°C at 760 mmHg
Flash Point:246.9°C
Density:1.25g/cm³
XLogP3:3.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:269.08743528
Heavy Atom Count:19
Complexity:346

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)NC1=C(C=C2C(=C1)CC3=CC=CC=C32)SC

Technology Process of n-[3-(Methylsulfanyl)-9h-fluoren-2-yl]acetamide

There total 14 articles about n-[3-(Methylsulfanyl)-9h-fluoren-2-yl]acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1115-47-5
N-acetyl-DL-methionine

: 6098-44-8
NA-AAF

: 6098-47-1
3-(methylthio)-2-acetamidofluorene

: 21879-09-4
1-(methylthio)-2-acetamidofluorene

Guidance literature:: With phosphate buffer; In ethanol; at 48 ℃; for 2.5h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/jm00148a014

Reference yield:

: 53-95-2
N-Hydroxy-2-acetylaminofluoren

: 6098-47-1
3-(methylthio)-2-acetamidofluorene

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / pyridine / 0.75 h / Ambient temperature

2: 0.1 M phosphate buffer (pH=7.8) / aq. ethanol / 2.5 h / 48 °C

With phosphate buffer; In pyridine; ethanol;
DOI:10.1021/jm00148a014

Reference yield:

: 16233-23-1
3-Methylmercapto-fluorenon

: 6098-47-1
3-(methylthio)-2-acetamidofluorene

Guidance literature:: Multi-step reaction with 9 steps

1: NO₂/HNO₃ / acetic acid

2: NO₂/HNO₃

3: aq. HBr / acetic acid

4: aq. N₂H₄ / bis-(2-hydroxy-ethyl) ether

5: benzene

6: (i) NO₂/HNO₃, HNO₃, (ii) aq. HBr, AcOH

7: aq. NaOH / ethanol

8: (i) aq. HCl, NaNO₂, (ii) H₃PO₂

9: (i) N₂H₄, Pd-C, (ii) /BRN= 385737/

With sodium hydroxide; hydrogen bromide; nitric acid; Nitrogen dioxide; hydrazine hydrate; In ethanol; acetic acid; diethylene glycol; benzene;
DOI:10.1021/jm00317a041