(2R,3S)-2-((R)-2-Acetoxy-3-phenyl-propionylamino)-3-hydroxy-4-methyl-pentanoic acid allyl ester

Base Information

Chemical Name:(2R,3S)-2-((R)-2-Acetoxy-3-phenyl-propionylamino)-3-hydroxy-4-methyl-pentanoic acid allyl ester
CAS No.:521304-56-3
Molecular Formula:C₂₀H₂₇NO₆
Molecular Weight:377.437
Hs Code.:

Synonyms:(2R,3S)-2-((R)-2-Acetoxy-3-phenyl-propionylamino)-3-hydroxy-4-methyl-pentanoic acid allyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3S)-2-((R)-2-Acetoxy-3-phenyl-propionylamino)-3-hydroxy-4-methyl-pentanoic acid allyl ester

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Technology Process of (2R,3S)-2-((R)-2-Acetoxy-3-phenyl-propionylamino)-3-hydroxy-4-methyl-pentanoic acid allyl ester

There total 1 articles about (2R,3S)-2-((R)-2-Acetoxy-3-phenyl-propionylamino)-3-hydroxy-4-methyl-pentanoic acid allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 146235-25-8
(2R)-2-acetoxy-3-phenylpropanoic acid

: allyl (2R,3S)-3-hydroxyleucinate

: 521304-56-3
(2R,3S)-2-((R)-2-Acetoxy-3-phenyl-propionylamino)-3-hydroxy-4-methyl-pentanoic acid allyl ester

Guidance literature:: With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran;
DOI:10.3987/COM-02-S24

Reference yield: 40.0%

: 521304-56-3
(2R,3S)-2-((R)-2-Acetoxy-3-phenyl-propionylamino)-3-hydroxy-4-methyl-pentanoic acid allyl ester

: 521304-51-8
(2S,3R,4S,5R)-3,4-Bis-benzyloxy-5-(4-methoxy-benzyloxy)-2-phenylsulfanyl-tetrahydro-pyran

: (2R,3S)-2-((R)-2-Acetoxy-3-phenyl-propionylamino)-3-[(2S,3R,4S,5R)-3,4-bis-benzyloxy-5-(4-methoxy-benzyloxy)-tetrahydro-pyran-2-yloxy]-4-methyl-pentanoic acid allyl ester

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; 4 A molecular sieve; In 1,2-dichloro-ethane; at 0 ℃;
DOI:10.3987/COM-02-S24

Reference yield:

: 521304-56-3
(2R,3S)-2-((R)-2-Acetoxy-3-phenyl-propionylamino)-3-hydroxy-4-methyl-pentanoic acid allyl ester

: 521304-52-9
(3R,4S,5R)-3,4-Bis-benzyloxy-2-fluoro-5-(4-methoxy-benzyloxy)-tetrahydro-pyran

: (2R,3S)-2-((R)-2-Acetoxy-3-phenyl-propionylamino)-3-[(2R,3R,4S,5R)-3,4-bis-benzyloxy-5-(4-methoxy-benzyloxy)-tetrahydro-pyran-2-yloxy]-4-methyl-pentanoic acid allyl ester

: (2R,3S)-2-((R)-2-Acetoxy-3-phenyl-propionylamino)-3-[(2S,3R,4S,5R)-3,4-bis-benzyloxy-5-(4-methoxy-benzyloxy)-tetrahydro-pyran-2-yloxy]-4-methyl-pentanoic acid allyl ester

Guidance literature:: With 4 A molecular sieve; silver perchlorate; tin(ll) chloride; In diethyl ether; at -20 - 20 ℃; Title compound not separated from byproducts;
DOI:10.3987/COM-02-S24