Technology Process of C28H36N2O2
There total 4 articles about C28H36N2O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 18 h / 20 °C
2.1: potassium carbonate / N,N-dimethyl-formamide / 6 h / 80 °C
3.1: palladium diacetate; tris-(o-tolyl)phosphine / acetonitrile / 6 h / 90 °C
4.1: sodium hydroxide / ethanol / 3 h / Reflux
4.2: 2 h / 40 °C
4.3: 1 h / 20 °C
With
palladium diacetate; potassium carbonate; tris-(o-tolyl)phosphine; sodium hydroxide;
In
ethanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.bmc.2013.05.035
- Guidance literature:
-
C25H31NO3;
With
sodium hydroxide;
In
ethanol;
for 3h;
Reflux;
With
thionyl chloride;
at 40 ℃;
for 2h;
piperidine;
In
dichloromethane;
at 20 ℃;
for 1h;
DOI:10.1016/j.bmc.2013.05.035
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 6 h / 80 °C
2.1: palladium diacetate; tris-(o-tolyl)phosphine / acetonitrile / 6 h / 90 °C
3.1: sodium hydroxide / ethanol / 3 h / Reflux
3.2: 2 h / 40 °C
3.3: 1 h / 20 °C
With
palladium diacetate; potassium carbonate; tris-(o-tolyl)phosphine; sodium hydroxide;
In
ethanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.bmc.2013.05.035