8-methoxycarbonyloctyl 6-O-<6-O-(4-O-acetyl-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-α-D-mannopyranosyl>-2,3,4-tri-O-benzyl-β-D-mannopyranoside

Base Information

Chemical Name:8-methoxycarbonyloctyl 6-O-<6-O-(4-O-acetyl-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-α-D-mannopyranosyl>-2,3,4-tri-O-benzyl-β-D-mannopyranoside
CAS No.:140182-89-4
Molecular Formula:C₉₄H₁₀₃NO₂₀
Molecular Weight:1566.85
Hs Code.:

8-methoxycarbonyloctyl 6-O-<6-O-(4-O-acetyl-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-α-D-mannopyranosyl>-2,3,4-tri-O-benzyl-β-D-mannopyranoside

Synonyms:8-methoxycarbonyloctyl 6-O-<6-O-(4-O-acetyl-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-α-D-mannopyranosyl>-2,3,4-tri-O-benzyl-β-D-mannopyranoside

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Chemical Property of 8-methoxycarbonyloctyl 6-O-<6-O-(4-O-acetyl-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-α-D-mannopyranosyl>-2,3,4-tri-O-benzyl-β-D-mannopyranoside

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Technology Process of 8-methoxycarbonyloctyl 6-O-<6-O-(4-O-acetyl-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-α-D-mannopyranosyl>-2,3,4-tri-O-benzyl-β-D-mannopyranoside

There total 1 articles about 8-methoxycarbonyloctyl 6-O-<6-O-(4-O-acetyl-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-α-D-mannopyranosyl>-2,3,4-tri-O-benzyl-β-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 140385-12-2
4-O-acetyl-3,6-di-O-benzyl-2-deoxy-2-phthalimido-α,β-D-glucopyranosyl chloride

: 140182-88-3
8-methoxycarbonyloctyl 2,3,4-tri-O-benzyl-6-O-(2,3,4-tri-O-benzyl-α-D-mannopyranosyl)-β-D-mannopyranoside

: 140182-89-4
8-methoxycarbonyloctyl 6-O-<6-O-(4-O-acetyl-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-α-D-mannopyranosyl>-2,3,4-tri-O-benzyl-β-D-mannopyranoside

Guidance literature:: With 2,4,6-trimethyl-pyridine; 4 A molecular sieve; silver trifluoromethanesulfonate; Yield given. Multistep reaction; 1.) CH₂Cl₂, -30 deg C, 10 min 2.) CH₂Cl₂, rt, 24 h;
DOI:10.1016/0008-6215(92)84095-A

Reference yield: 87.0%

: 140182-89-4
8-methoxycarbonyloctyl 6-O-<6-O-(4-O-acetyl-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-α-D-mannopyranosyl>-2,3,4-tri-O-benzyl-β-D-mannopyranoside

: 140182-90-7
8-methoxycarbonyloctyl 2,3,4-tri-O-benzyl-6-O-<2,3,4-tri-O-benzyl-6-O-(3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-α-D-mannopyranosyl>-β-D-mannopyranoside

Guidance literature:: With sodium methylate; In methanol; for 4h; Ambient temperature;
DOI:10.1016/0008-6215(92)84095-A

Reference yield:

: 108-24-7
acetic anhydride

: 140182-89-4
8-methoxycarbonyloctyl 6-O-<6-O-(4-O-acetyl-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-α-D-mannopyranosyl>-2,3,4-tri-O-benzyl-β-D-mannopyranoside

: 140182-91-8
8-methoxycarbonyl 6-O-<6-O-(2-acetamido-4-O-acetyl-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-2,3,4-tri-O-benzyl-α-D-mannopyranosyl>-2,3,4-tri-O-benzyl-β-D-mannopyranoside

Guidance literature:: With pyridine; hydrazinium monoacetate; Yield given. Multistep reaction; 1.) MeOH, reflux, 23 h 2.) rt, 16 h;
DOI:10.1016/0008-6215(92)84095-A