Benzoic acid (1S,2S,3S,6S,7R)-5-oxo-4-oxa-tricyclo[4.2.1.0^3,7]non-2-yl ester

Base Information

• Chemical Name: Benzoic acid (1S,2S,3S,6S,7R)-5-oxo-4-oxa-tricyclo[4.2.1.0^3,7]non-2-yl ester
• CAS No.: 77299-91-3
• Molecular Formula: C₁₅H₁₄O₄
• Molecular Weight: 258.274

Synonyms:Benzoic acid (1S,2S,3S,6S,7R)-5-oxo-4-oxa-tricyclo[4.2.1.0^3,7]non-2-yl ester

Chemical Property of Benzoic acid (1S,2S,3S,6S,7R)-5-oxo-4-oxa-tricyclo[4.2.1.0^3,7]non-2-yl ester

Chemical Property:

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Technology Process of Benzoic acid (1S,2S,3S,6S,7R)-5-oxo-4-oxa-tricyclo[4.2.1.0^3,7]non-2-yl ester

There total 1 articles about Benzoic acid (1S,2S,3S,6S,7R)-5-oxo-4-oxa-tricyclo[4.2.1.0^3,7]non-2-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

dioxa-3,5 exo phenyl-4 syn carbomethoxy-9 endo tricyclo <5.2.1.02,6> decane (68763-55-3,68831-99-2,68832-01-9,68832-02-0) → Benzoic acid (1S,2S,3S,6S,7R)-5-oxo-4-oxa-tricyclo[4.2.1.03,7]non-2-yl ester (77299-91-3)

Guidance literature:

With N-Bromosuccinimide; Perbenzoic acid; barium carbonate; In tetrachloromethane; for 1.25h; Heating;

DOI:10.1016/0040-4020(80)80151-7

Reference yield: 64.0%

Benzoic acid (1S,2S,3S,6S,7R)-5-oxo-4-oxa-tricyclo[4.2.1.03,7]non-2-yl ester (77299-91-3) → 5,6-Dihydroxybicyclo<2.2.1>octane-2-carboxylic acid-γ-lactone (16479-72-4,92343-46-9)

Guidance literature:

With soude aqueuse; In methanol; Ambient temperature;

DOI:10.1016/0040-4020(80)80151-7

upstream raw materials:

dioxa-3,5 exo phenyl-4 syn carbomethoxy-9 endo tricyclo <5.2.1.0^2,6> decane

Downstream raw materials:

5,6-Dihydroxybicyclo<2.2.1>octane-2-carboxylic acid-γ-lactone

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