2-nitro-2-phenylhydrazonoacetamide oxime

Base Information

• Chemical Name: 2-nitro-2-phenylhydrazonoacetamide oxime
• CAS No.: 152574-42-0
• Molecular Formula: C₈H₉N₅O₃
• Molecular Weight: 223.191
• Mol file: 152574-42-0.mol

Synonyms:2-nitro-2-phenylhydrazonoacetamide oxime

Chemical Property of 2-nitro-2-phenylhydrazonoacetamide oxime

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 2-nitro-2-phenylhydrazonoacetamide oxime

There total 1 articles about 2-nitro-2-phenylhydrazonoacetamide oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

2-nitro-2-phenylhydrazonoacetonitrile (35509-32-1) → 2-nitro-2-phenylhydrazonoacetamide oxime (152574-42-0)

Guidance literature:

With hydroxylamine; In isopropyl alcohol; at 50 ℃; for 2h;

Reference yield: 65.0%

2-nitro-2-phenylhydrazonoacetamide oxime (152574-42-0) → 5-amino-4-nitro-2-phenyl-1,2,3-triazole (152574-43-1)

Guidance literature:

With urea; at 140 ℃; for 0.333333h;

Reference yield:

2-nitro-2-phenylhydrazonoacetamide oxime (152574-42-0) → 4,5-diamino-2-phenyl-{1,2,3}triazole (53543-28-5)

Guidance literature:

Multi-step reaction with 3 steps

1: 79 percent / acetic acid / 0.5 h / 50 °C

2: 43 percent / K₂CO₃ / 150 °C / 0.02 - 0.04 Torr

3: 51 percent / aq. HCl, Zn / ethanol / 1 h / Heating

With hydrogenchloride; potassium carbonate; acetic acid; zinc; In ethanol;

upstream raw materials:

2-nitro-2-phenylhydrazonoacetonitrile

Downstream raw materials:

5-amino-4-nitro-2-phenyl-1,2,3-triazole

4,5-diamino-2-phenyl-{1,2,3}triazole