2-nitrophenyl O-<3,4-O-isopropylidene-2-O-(4-methoxybenzyl)-α-L-fucopyranosyl>-(1->3)-O-(2-acetamido-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranosyl)-(1->6)-2-acetamido-2-deoxy-3,4-O-isopropylidene-α-D-galactopyranoside

Base Information

Chemical Name:2-nitrophenyl O-<3,4-O-isopropylidene-2-O-(4-methoxybenzyl)-α-L-fucopyranosyl>-(1->3)-O-(2-acetamido-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranosyl)-(1->6)-2-acetamido-2-deoxy-3,4-O-isopropylidene-α-D-galactopyranoside
CAS No.:142329-82-6
Molecular Formula:C₄₅H₆₁N₃O₁₈
Molecular Weight:931.989
Hs Code.:

2-nitrophenyl O-<3,4-O-isopropylidene-2-O-(4-methoxybenzyl)-α-L-fucopyranosyl>-(1->3)-O-(2-acetamido-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranosyl)-(1->6)-2-acetamido-2-deoxy-3,4-O-isopropylidene-α-D-galactopyranoside

Synonyms:2-nitrophenyl O-<3,4-O-isopropylidene-2-O-(4-methoxybenzyl)-α-L-fucopyranosyl>-(1->3)-O-(2-acetamido-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranosyl)-(1->6)-2-acetamido-2-deoxy-3,4-O-isopropylidene-α-D-galactopyranoside

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Chemical Property of 2-nitrophenyl O-<3,4-O-isopropylidene-2-O-(4-methoxybenzyl)-α-L-fucopyranosyl>-(1->3)-O-(2-acetamido-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranosyl)-(1->6)-2-acetamido-2-deoxy-3,4-O-isopropylidene-α-D-galactopyranoside

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Technology Process of 2-nitrophenyl O-<3,4-O-isopropylidene-2-O-(4-methoxybenzyl)-α-L-fucopyranosyl>-(1->3)-O-(2-acetamido-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranosyl)-(1->6)-2-acetamido-2-deoxy-3,4-O-isopropylidene-α-D-galactopyranoside

There total 4 articles about 2-nitrophenyl O-<3,4-O-isopropylidene-2-O-(4-methoxybenzyl)-α-L-fucopyranosyl>-(1->3)-O-(2-acetamido-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranosyl)-(1->6)-2-acetamido-2-deoxy-3,4-O-isopropylidene-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 130572-02-0
Methyl 3,4-O-Isopropylidene-2-O-(4-methoxybenzyl)-1-Thio-β-L-Fucopyranoside

: 142329-81-5
2-nitrophenyl O-(2-acetamido-2-deoxy-4,6-O-isopyropylidene-β-D-glucopyranosyl)-(1->6)-2-acetamido-2-deoxy-3,4-O-isopropylidene-α-D-galactopyranoside

: 142329-82-6
2-nitrophenyl O-<3,4-O-isopropylidene-2-O-(4-methoxybenzyl)-α-L-fucopyranosyl>-(1->3)-O-(2-acetamido-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranosyl)-(1->6)-2-acetamido-2-deoxy-3,4-O-isopropylidene-α-D-galactopyranoside

Guidance literature:: With 4 A molecular sieve; tetrabutylammomium bromide; copper(ll) bromide; In 1,2-dichloro-ethane; N,N-dimethyl-formamide; Ambient temperature;
DOI:10.1016/S0008-6215(00)90562-7

Reference yield:

: 130572-04-2
methyl 3,4-O-isopropylidene-1-thio-β-L-fucopyranoside

: 142329-82-6
2-nitrophenyl O-<3,4-O-isopropylidene-2-O-(4-methoxybenzyl)-α-L-fucopyranosyl>-(1->3)-O-(2-acetamido-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranosyl)-(1->6)-2-acetamido-2-deoxy-3,4-O-isopropylidene-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DMF, r.t., 0.5 h, then cooled, 2.) r.t., 2 h

2: 94 percent / tetrabutylammonium bromide, CuBr₂, molecular sieves 4 Angstroem / 1,2-dichloro-ethane; dimethylformamide / Ambient temperature

With 4 A molecular sieve; tetrabutylammomium bromide; sodium hydride; copper(ll) bromide; In 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)90562-7

Reference yield:

: 124040-71-7
2-nitrophenyl O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-(1->6)-2-acetamido-2-deoxy-α-D-galactopyranoside

: 142329-82-6
2-nitrophenyl O-<3,4-O-isopropylidene-2-O-(4-methoxybenzyl)-α-L-fucopyranosyl>-(1->3)-O-(2-acetamido-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranosyl)-(1->6)-2-acetamido-2-deoxy-3,4-O-isopropylidene-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / 4-toluenesulfonic acid monohydrate / dimethylformamide / 3 h / 70 °C

2: 94 percent / tetrabutylammonium bromide, CuBr₂, molecular sieves 4 Angstroem / 1,2-dichloro-ethane; dimethylformamide / Ambient temperature

With 4 A molecular sieve; p-toluenesulfonic acid monohydrate; tetrabutylammomium bromide; copper(ll) bromide; In 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)90562-7