N₁-(4-{[(2,4-dichlorophenyl)sulfonyl]amino}butyl)-N₂-{[(1,1-dimethylethyl)oxy]carbonyl}-L-leucinamide

Base Information

• Chemical Name: N₁-(4-{[(2,4-dichlorophenyl)sulfonyl]amino}butyl)-N₂-{[(1,1-dimethylethyl)oxy]carbonyl}-L-leucinamide
• CAS No.: 929281-67-4
• Molecular Formula: C₂₁H₃₃Cl₂N₃O₅S
• Molecular Weight: 510.482

Synonyms:N₁-(4-{[(2,4-dichlorophenyl)sulfonyl]amino}butyl)-N₂-{[(1,1-dimethylethyl)oxy]carbonyl}-L-leucinamide

Chemical Property of N₁-(4-{[(2,4-dichlorophenyl)sulfonyl]amino}butyl)-N₂-{[(1,1-dimethylethyl)oxy]carbonyl}-L-leucinamide

Chemical Property:

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Technology Process of N₁-(4-{[(2,4-dichlorophenyl)sulfonyl]amino}butyl)-N₂-{[(1,1-dimethylethyl)oxy]carbonyl}-L-leucinamide

There total 1 articles about N₁-(4-{[(2,4-dichlorophenyl)sulfonyl]amino}butyl)-N₂-{[(1,1-dimethylethyl)oxy]carbonyl}-L-leucinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

N-(4-aminobutyl)-2,4-dichlorobenzenesulfonamide (929281-65-2) + N-tert-butoxycarbonyl-L-leucine (13139-15-6,53296-34-7) → N1-(4-{[(2,4-dichlorophenyl)sulfonyl]amino}butyl)-N2-{[(1,1-dimethylethyl)oxy]carbonyl}-L-leucinamide (929281-67-4)

Guidance literature:

N-(4-aminobutyl)-2,4-dichlorobenzenesulfonamide; N-tert-butoxycarbonyl-L-leucine; With 4-methyl-morpholine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-hydroxy-3,4-dihydrobenzotriazine-4-one; In dichloromethane; at 0 - 20 ℃;

at 0 ℃;

Reference yield: 100.0%

N1-(4-{[(2,4-dichlorophenyl)sulfonyl]amino}butyl)-N2-{[(1,1-dimethylethyl)oxy]carbonyl}-L-leucinamide (929281-67-4) → N-(4-{[(2,4-dichlorophenyl)sulfonyl]amino}butyl)-L-leucinamide hydrochloride (929281-69-6)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; methanol; at 20 ℃; for 2h; Product distribution / selectivity;

upstream raw materials:

N-(4-aminobutyl)-2,4-dichlorobenzenesulfonamide

N-tert-butoxycarbonyl-L-leucine

Downstream raw materials:

N-(4-{[(2,4-dichlorophenyl)sulfonyl]amino}butyl)-L-leucinamide hydrochloride

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