Technology Process of C15H21N3O2
There total 3 articles about C15H21N3O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
n-Octyl anthranilate;
With
hydrogenchloride; sodium nitrite;
In
water; acetone;
at 0 ℃;
With
sodium azide; sodium acetate;
In
water; acetone;
at 5 ℃;
DOI:10.1016/j.carres.2012.08.001
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydride / mineral oil; toluene / 2 h / Reflux; Inert atmosphere
2.1: hydrogenchloride; sodium nitrite / water; acetone / 0 °C
2.2: 5 °C
With
hydrogenchloride; sodium hydride; sodium nitrite;
In
water; acetone; toluene; mineral oil;
DOI:10.1016/j.carres.2012.08.001
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydride / mineral oil; toluene / 2 h / Reflux; Inert atmosphere
2.1: hydrogenchloride; sodium nitrite / water; acetone / 0 °C
2.2: 5 °C
With
hydrogenchloride; sodium hydride; sodium nitrite;
In
water; acetone; toluene; mineral oil;
DOI:10.1016/j.carres.2012.08.001