bis(p-fluorophenyl)tin dibromide

Base Information

Chemical Name:bis(p-fluorophenyl)tin dibromide
CAS No.:156868-10-9
Molecular Formula:C₁₂H₈Br₂F₂Sn
Molecular Weight:468.71
Hs Code.:

Synonyms:bis(p-fluorophenyl)tin dibromide

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Chemical Property of bis(p-fluorophenyl)tin dibromide

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Technology Process of bis(p-fluorophenyl)tin dibromide

There total 1 articles about bis(p-fluorophenyl)tin dibromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1251-03-2
tetrakis(4-fluorophenyl)stannane

: 7789-67-5
stannic bromide

: 156868-10-9
bis(p-fluorophenyl)tin dibromide

Guidance literature:: In neat (no solvent); slow heating of a mixt. of Sn-compd. and SnBr4 to 170-180°C under N2, keeping at this temp. for 2 h; dissolution of resulting oil in hexane, removing slight turbidity by filtn., cooling to -78°C, filtn., rapidly washing with cold hexane, evapn. of mother liquor yields second crop, elem. anal.;
DOI:10.1016/0022-328X(94)80033-2

Reference yield: 98.0%

: 156868-10-9
bis(p-fluorophenyl)tin dibromide

: (DMSO)2bis(p-fluorophenyl)tin dibromide

Guidance literature:: With DMSO; In toluene; combining cold (0°C) solns. of DMSO in toluene and tin-compd. in the same solvent under N2, pptn.; filtn., washing with pentane, drying in vacuo, elem. anal.;
DOI:10.1016/0022-328X(94)80033-2

Reference yield: 82.0%

: 7117-41-1
thiirane 1-oxide

: 156868-10-9
bis(p-fluorophenyl)tin dibromide

: bis(thiirane-1-oxide)bis(p-fluorophenyl)tin dibromide

Guidance literature:: In toluene; combining cold (0°C) solns. of thiirane-1-oxide in toluene and tin-compd. in the same solvent under N2; pptn. by addn. of n-hexane, filtn., washing with cold n-hexane, drying in vacuo, elem. anal.;
DOI:10.1016/0022-328X(94)80033-2