C₃₀H₄₀N₄O₃Si

Base Information

Chemical Name:C₃₀H₄₀N₄O₃Si
CAS No.:1431702-88-3
Molecular Formula:C₃₀H₄₀N₄O₃Si
Molecular Weight:532.758
Hs Code.:

C<sub>30</sub>H<sub>40</sub>N<sub>4</sub>O<sub>3</sub>Si

Synonyms:C₃₀H₄₀N₄O₃Si

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Chemical Property of C₃₀H₄₀N₄O₃Si

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Technology Process of C₃₀H₄₀N₄O₃Si

There total 5 articles about C₃₀H₄₀N₄O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1346245-14-4
C₂₅H₃₄ClN₃O₃Si

: 1431702-88-3
C₃₀H₄₀N₄O₃Si

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 12 h / 100 °C / Inert atmosphere

2: potassium tert-butylate; 18-crown-6 ether / dimethyl sulfoxide / 1.5 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; 18-crown-6 ether; potassium tert-butylate; sodium carbonate; In 1,2-dimethoxyethane; water; dimethyl sulfoxide;

Reference yield:

: 82031-32-1
7-bromo-1H-quinoxalin-2-one

: 1431702-88-3
C₃₀H₄₀N₄O₃Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium t-butanolate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; palladium diacetate / 1,2-dimethoxyethane / 5 h / Inert atmosphere; Reflux

2.1: trichlorophosphate / 0.67 h / 80 °C

3.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 5 °C / Inert atmosphere

3.2: 5 h / 5 - 20 °C / Inert atmosphere

4.1: sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 12 h / 100 °C / Inert atmosphere

5.1: potassium tert-butylate; 18-crown-6 ether / dimethyl sulfoxide / 1.5 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; 18-crown-6 ether; potassium tert-butylate; palladium diacetate; sodium hydride; sodium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate; trichlorophosphate; In 1,2-dimethoxyethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 10272-07-8
3.5-dimethoxyaniline

: 1431702-88-3
C₃₀H₄₀N₄O₃Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium t-butanolate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; palladium diacetate / 1,2-dimethoxyethane / 5 h / Inert atmosphere; Reflux

2.1: trichlorophosphate / 0.67 h / 80 °C

3.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 5 °C / Inert atmosphere

3.2: 5 h / 5 - 20 °C / Inert atmosphere

4.1: sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 12 h / 100 °C / Inert atmosphere

5.1: potassium tert-butylate; 18-crown-6 ether / dimethyl sulfoxide / 1.5 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; 18-crown-6 ether; potassium tert-butylate; palladium diacetate; sodium hydride; sodium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate; trichlorophosphate; In 1,2-dimethoxyethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;