N₁-[3-(4-chlorophenyl)-1,2,4-oxadiazol-5-ylcarbonyl]-N₄-phenyl thiosemicarbazide

Base Information

• Chemical Name: N₁-[3-(4-chlorophenyl)-1,2,4-oxadiazol-5-ylcarbonyl]-N₄-phenyl thiosemicarbazide
• CAS No.: 1187736-27-1
• Molecular Formula: C₁₆H₁₂ClN₅O₂S
• Molecular Weight: 373.823

Synonyms:N₁-[3-(4-chlorophenyl)-1,2,4-oxadiazol-5-ylcarbonyl]-N₄-phenyl thiosemicarbazide

Chemical Property of N₁-[3-(4-chlorophenyl)-1,2,4-oxadiazol-5-ylcarbonyl]-N₄-phenyl thiosemicarbazide

Chemical Property:

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Technology Process of N₁-[3-(4-chlorophenyl)-1,2,4-oxadiazol-5-ylcarbonyl]-N₄-phenyl thiosemicarbazide

There total 1 articles about N₁-[3-(4-chlorophenyl)-1,2,4-oxadiazol-5-ylcarbonyl]-N₄-phenyl thiosemicarbazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

3-(4-chlorophenyl)-1,2,4-oxadiazole-5-carbohydrazide (861146-17-0) + phenyl isothiocyanate (103-72-0) → 5-[3-(4-chlorophenyl)-1,2,4-oxadiazol-5-yl]-2-(N-phenylamino)-1,3,4-oxadiazole (1187736-35-1) + N1-[3-(4-chlorophenyl)-1,2,4-oxadiazol-5-ylcarbonyl]-N4-phenyl thiosemicarbazide (1187736-27-1)

Guidance literature:

In tetrahydrofuran; for 0.5h; Inert atmosphere; Reflux;

DOI:10.1002/jhet.133

Reference yield: 90.0%

N1-[3-(4-chlorophenyl)-1,2,4-oxadiazol-5-ylcarbonyl]-N4-phenyl thiosemicarbazide (1187736-27-1) → 5-[3-(4-chlorophenyl)-1,2,4-oxadiazol-5-yl]-2-(N-phenylamino)-1,3,4-oxadiazole (1187736-35-1)

Guidance literature:

With dicyclohexyl-carbodiimide; In tetrahydrofuran; for 2h; Inert atmosphere; Reflux;

DOI:10.1002/jhet.133

upstream raw materials:

3-(4-chlorophenyl)-1,2,4-oxadiazole-5-carbohydrazide

phenyl isothiocyanate

Downstream raw materials:

5-[3-(4-chlorophenyl)-1,2,4-oxadiazol-5-yl]-2-(N-phenylamino)-1,3,4-oxadiazole

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