5-adamantan-1-yl-N-(3,4-dihydroxybenzyl)-2-hydroxy-4-methoxy-benzoic acid amide

Base Information

Chemical Name:5-adamantan-1-yl-N-(3,4-dihydroxybenzyl)-2-hydroxy-4-methoxy-benzoic acid amide
CAS No.:1422043-81-9
Molecular Formula:C₂₅H₂₉NO₅
Molecular Weight:423.509
Hs Code.:

Synonyms:5-adamantan-1-yl-N-(3,4-dihydroxybenzyl)-2-hydroxy-4-methoxy-benzoic acid amide

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Chemical Property of 5-adamantan-1-yl-N-(3,4-dihydroxybenzyl)-2-hydroxy-4-methoxy-benzoic acid amide

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Technology Process of 5-adamantan-1-yl-N-(3,4-dihydroxybenzyl)-2-hydroxy-4-methoxy-benzoic acid amide

There total 5 articles about 5-adamantan-1-yl-N-(3,4-dihydroxybenzyl)-2-hydroxy-4-methoxy-benzoic acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₂H₂₅NO₆

: 1124-40-9
3,4-dihydroxybenzylamine hydrochloride

: 1422043-81-9
5-adamantan-1-yl-N-(3,4-dihydroxybenzyl)-2-hydroxy-4-methoxy-benzoic acid amide

Guidance literature:: With sodium hydrogencarbonate; In water; at 60 ℃; Inert atmosphere;
DOI:10.1016/j.bmcl.2013.11.056

Reference yield:

: 135078-29-4
C₁₈H₂₂O₄

: 1422043-81-9
5-adamantan-1-yl-N-(3,4-dihydroxybenzyl)-2-hydroxy-4-methoxy-benzoic acid amide

Guidance literature:: Multi-step reaction with 2 steps

1: dicyclohexyl-carbodiimide / 1,4-dioxane / 12 h / 20 °C / Inert atmosphere

2: sodium hydrogencarbonate / water / 60 °C / Inert atmosphere

With sodium hydrogencarbonate; dicyclohexyl-carbodiimide; In 1,4-dioxane; water;
DOI:10.1016/j.bmcl.2013.11.056

Reference yield:

: 2237-36-7
4-methoxysalicylic acid

: 1422043-81-9
5-adamantan-1-yl-N-(3,4-dihydroxybenzyl)-2-hydroxy-4-methoxy-benzoic acid amide

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid; acetic acid / dichloromethane / 20 °C

2: dicyclohexyl-carbodiimide / 1,4-dioxane / 12 h / 20 °C / Inert atmosphere

3: sodium hydrogencarbonate / water / 60 °C / Inert atmosphere

With sulfuric acid; sodium hydrogencarbonate; acetic acid; dicyclohexyl-carbodiimide; In 1,4-dioxane; dichloromethane; water;
DOI:10.1016/j.bmcl.2013.11.056