3-(3-methyl-4-oxo-7-phenyl-4H-isoxazolo[4,5-d]pyridazin-5-yl)propionic acid

Base Information

• Chemical Name: 3-(3-methyl-4-oxo-7-phenyl-4H-isoxazolo[4,5-d]pyridazin-5-yl)propionic acid
• CAS No.: 923569-72-6
• Molecular Formula: C₁₅H₁₃N₃O₄
• Molecular Weight: 299.286

Synonyms:3-(3-methyl-4-oxo-7-phenyl-4H-isoxazolo[4,5-d]pyridazin-5-yl)propionic acid

Chemical Property of 3-(3-methyl-4-oxo-7-phenyl-4H-isoxazolo[4,5-d]pyridazin-5-yl)propionic acid

Chemical Property:

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Technology Process of 3-(3-methyl-4-oxo-7-phenyl-4H-isoxazolo[4,5-d]pyridazin-5-yl)propionic acid

There total 2 articles about 3-(3-methyl-4-oxo-7-phenyl-4H-isoxazolo[4,5-d]pyridazin-5-yl)propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C17H17N3O4 (1027087-89-3) → 3-(3-methyl-4-oxo-7-phenyl-4H-isoxazolo[4,5-d]pyridazin-5-yl)propionic acid (923569-72-6)

Guidance literature:

With sodium hydroxide; In ethanol; at 20 ℃; for 15h;

DOI:10.1021/jm060743g

Reference yield:

3-Methyl-7-phenyl-5H-isoxazolo[4,5-d]pyridazin-4-one (129663-23-6) → 3-(3-methyl-4-oxo-7-phenyl-4H-isoxazolo[4,5-d]pyridazin-5-yl)propionic acid (923569-72-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 70 percent / K₂CO₃ / dimethylformamide / 15 h / 20 °C

2: aq. NaOH / ethanol / 15 h / 20 °C

With sodium hydroxide; potassium carbonate; In ethanol; N,N-dimethyl-formamide;

DOI:10.1021/jm060743g

Reference yield:

3-(3-methyl-4-oxo-7-phenyl-4H-isoxazolo[4,5-d]pyridazin-5-yl)propionic acid (923569-72-6) → C15H12ClN3O3

Guidance literature:

With thionyl chloride; triethylamine; at 60 ℃; for 2h;

DOI:10.1021/jm060743g

upstream raw materials:

C₁₇H₁₇N₃O₄

3-Methyl-7-phenyl-5H-isoxazolo[4,5-d]pyridazin-4-one

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