C₅₈H₉₇N₃O₁₇

Base Information

Chemical Name:C₅₈H₉₇N₃O₁₇
CAS No.:1609184-38-4
Molecular Formula:C₅₈H₉₇N₃O₁₇
Molecular Weight:1108.42
Hs Code.:

C<sub>58</sub>H<sub>97</sub>N<sub>3</sub>O<sub>17</sub>

Synonyms:C₅₈H₉₇N₃O₁₇

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Chemical Property of C₅₈H₉₇N₃O₁₇

Chemical Property:

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Technology Process of C₅₈H₉₇N₃O₁₇

There total 18 articles about C₅₈H₉₇N₃O₁₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1374760-32-3
C₃₄H₅₉N₃O₁₄

: 474-25-9
chenodeoxycholic acid

: 1609184-38-4
C₅₈H₉₇N₃O₁₇

Guidance literature:: chenodeoxycholic acid; With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 ℃; for 0.166667h;

C₃₄H₅₉N₃O₁₄; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

Reference yield:

: 1374760-20-9
C₁₆H₃₀O₄Si

: 1609184-38-4
C₅₈H₉₇N₃O₁₇

Guidance literature:: Multi-step reaction with 11 steps

1.1: tetraethylammonium bromide / dichloromethane; N,N-dimethyl-formamide / 1 h / 20 °C / Molecular sieve; Inert atmosphere

1.2: 18 h / 20 °C / Inert atmosphere; Cooling with ice

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 15 h / 20 °C

3.1: dichloromethane / 0.5 h / 20 °C / Molecular sieve

3.2: 2 h / 0 °C

4.1: methanol; sodium methylate / 2 h

5.1: triethylamine / acetonitrile / 1.33 h / 0 °C

6.1: di(n-butyl)tin oxide / methanol / 2 h / Reflux

6.2: 20 °C

7.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-n-butyl-tin hydride / dichloromethane / 1 h / 20 °C

8.1: palladium 10% on activated carbon; hydrogen; acetic acid / water; 1,4-dioxane / 5 h / 20 °C / 1034.32 Torr

9.1: methanol; sodium methylate / 4 h

10.1: 8 h / 80 °C

11.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.17 h / 0 °C

11.2: 2 h / 20 °C

With methanol; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; tetraethylammonium bromide; tetrabutyl ammonium fluoride; hydrogen; tri-n-butyl-tin hydride; sodium methylate; di(n-butyl)tin oxide; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 127943-95-7
methyl (1R,3R)-3-(tert-butyldimethylsilyloxy)cyclohex-4-ene-1-carboxylate

: 1609184-38-4
C₅₈H₉₇N₃O₁₇

Guidance literature:: Multi-step reaction with 13 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / 0 °C / Inert atmosphere

2.2: 0.5 h / -20 °C / Inert atmosphere

3.1: tetraethylammonium bromide / dichloromethane; N,N-dimethyl-formamide / 1 h / 20 °C / Molecular sieve; Inert atmosphere

3.2: 18 h / 20 °C / Inert atmosphere; Cooling with ice

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 15 h / 20 °C

5.1: dichloromethane / 0.5 h / 20 °C / Molecular sieve

5.2: 2 h / 0 °C

6.1: methanol; sodium methylate / 2 h

7.1: triethylamine / acetonitrile / 1.33 h / 0 °C

8.1: di(n-butyl)tin oxide / methanol / 2 h / Reflux

8.2: 20 °C

9.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-n-butyl-tin hydride / dichloromethane / 1 h / 20 °C

10.1: palladium 10% on activated carbon; hydrogen; acetic acid / water; 1,4-dioxane / 5 h / 20 °C / 1034.32 Torr

11.1: methanol; sodium methylate / 4 h

12.1: 8 h / 80 °C

13.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.17 h / 0 °C

13.2: 2 h / 20 °C

With methanol; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; palladium 10% on activated carbon; tetraethylammonium bromide; tetrabutyl ammonium fluoride; hydrogen; tri-n-butyl-tin hydride; sodium methylate; di(n-butyl)tin oxide; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; 1,4-dioxane; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;