Technology Process of C20H24N4O7
There total 10 articles about C20H24N4O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium hydroxide monohydrate; water;
In
tetrahydrofuran;
at 0 ℃;
for 1h;
DOI:10.1039/c2cc36566a
- Guidance literature:
-
Multi-step reaction with 3 steps
1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol
2: hydrogen; palladium 10% on activated carbon / ethyl acetate; methanol / 760.05 Torr
3: lithium hydroxide monohydrate; water / tetrahydrofuran / 1 h / 0 °C
With
copper(ll) sulfate pentahydrate; lithium hydroxide monohydrate; palladium 10% on activated carbon; water; hydrogen; sodium L-ascorbate;
In
tetrahydrofuran; methanol; water; ethyl acetate; tert-butyl alcohol;
DOI:10.1039/c2cc36566a
- Guidance literature:
-
Multi-step reaction with 10 steps
1: iodine; triphenylphosphine; 1H-imidazole / toluene / 18 h / Reflux
2: sodium azide / N,N-dimethyl-formamide / 105 °C
3: palladium 10% on activated carbon
4: sodium hydrogencarbonate / water; methanol
5: water; acetic acid
6: sodium periodate / water; methanol
7: potassium carbonate / methanol
8: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol
9: hydrogen; palladium 10% on activated carbon / ethyl acetate; methanol / 760.05 Torr
10: lithium hydroxide monohydrate; water / tetrahydrofuran / 1 h / 0 °C
With
1H-imidazole; sodium periodate; sodium azide; copper(ll) sulfate pentahydrate; lithium hydroxide monohydrate; palladium 10% on activated carbon; water; hydrogen; iodine; sodium hydrogencarbonate; potassium carbonate; acetic acid; sodium L-ascorbate; triphenylphosphine;
In
tetrahydrofuran; methanol; water; ethyl acetate; N,N-dimethyl-formamide; toluene; tert-butyl alcohol;
DOI:10.1039/c2cc36566a