dibenzyl 1-methyl-6,9,10-triphenyl-cis-transoid-1,2-cis-2-7-8-diazatricyclo<4,2,2,0>deca-3,9-diene-7,8-dicarboxylate

Base Information

Chemical Name:dibenzyl 1-methyl-6,9,10-triphenyl-cis-transoid-1,2-cis-2-7-8-diazatricyclo<4,2,2,0>deca-3,9-diene-7,8-dicarboxylate
CAS No.:67723-27-7
Molecular Formula:C₄₃H₃₆N₂O₄
Molecular Weight:644.77
Hs Code.:

Synonyms:dibenzyl 1-methyl-6,9,10-triphenyl-cis-transoid-1,2-cis-2-7-8-diazatricyclo<4,2,2,0>deca-3,9-diene-7,8-dicarboxylate

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Chemical Property of dibenzyl 1-methyl-6,9,10-triphenyl-cis-transoid-1,2-cis-2-7-8-diazatricyclo<4,2,2,0>deca-3,9-diene-7,8-dicarboxylate

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Technology Process of dibenzyl 1-methyl-6,9,10-triphenyl-cis-transoid-1,2-cis-2-7-8-diazatricyclo<4,2,2,0>deca-3,9-diene-7,8-dicarboxylate

There total 1 articles about dibenzyl 1-methyl-6,9,10-triphenyl-cis-transoid-1,2-cis-2-7-8-diazatricyclo<4,2,2,0>deca-3,9-diene-7,8-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 2449-05-0
dibenzyl azodicarboxylate

: 67654-21-1,79491-03-5
bicyclo<4,2,0>octa-2,4,7-triene

: 67723-27-7
dibenzyl 1-methyl-6,9,10-triphenyl-cis-transoid-1,2-cis-2-7-8-diazatricyclo<4,2,2,0>deca-3,9-diene-7,8-dicarboxylate

Guidance literature:: In chloroform; for 120h; Ambient temperature;

Reference yield: 77.0%

: 67723-27-7
dibenzyl 1-methyl-6,9,10-triphenyl-cis-transoid-1,2-cis-2-7-8-diazatricyclo<4,2,2,0>deca-3,9-diene-7,8-dicarboxylate

: 67723-28-8
dibenzyl 1-methyl-7,10,11-triphenyl-cis-transoid-1,2-cis-2-transoid-2,3-cis-3-8,9-diaza-4-oxatetracyclo<5,2,2,0,0>undec-10-ene-8,9-dicarboxylate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In chloroform; for 4.5h; Heating;

Reference yield:

: 67723-27-7
dibenzyl 1-methyl-6,9,10-triphenyl-cis-transoid-1,2-cis-2-7-8-diazatricyclo<4,2,2,0>deca-3,9-diene-7,8-dicarboxylate

: 67723-29-9,79548-32-6
2-methyl-3,4,5-triphenyl-cis-transoid-1,9-cis-7,8-oxatricyclo<4,3,0,0>nona-2,4-diene

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / 3-chloroperbenzoic acid / CHCl₃ / 4.5 h / Heating

2: 2.) red mercuric oxide / 1.) 10 percent palladium on charcoal / 1.) ethyl acetate, RT, 2.) ethyl acetate, 22 h

With 3-chloro-benzenecarboperoxoic acid; mercury(II) oxide; palladium on activated charcoal; In chloroform;