2-nitrophenyl dimethylcarbamate

Base Information

• Chemical Name: 2-nitrophenyl dimethylcarbamate
• CAS No.: 3373-86-2
• Molecular Formula: C9H10 N2 O4
• Molecular Weight: 210.189
• Hs Code.: 2924299090
• Mol file: 3373-86-2.mol

Synonyms:Carbamicacid, dimethyl-, o-nitrophenyl ester (6CI,7CI,8CI); 2-NitrophenylN,N-dimethylcarbamate

Chemical Property of 2-nitrophenyl dimethylcarbamate

Chemical Property:

• Vapor Pressure: 0.000296mmHg at 25°C
• Boiling Point: 321.5°Cat760mmHg
• Flash Point: 148.2°C
• PSA: 75.36000
• Density: 1.292g/cm³
• LogP: 2.17840

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-nitrophenyl dimethylcarbamate

There total 3 articles about 2-nitrophenyl dimethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

2-hydroxynitrobenzene (88-75-5,78813-12-4) + N,N-Dimethylcarbamoyl chloride (79-44-7) → o-nitrophenyl-N,N-dimethylcarbamate (3373-86-2)

Guidance literature:

With 4-(dimethylamino)pyridine hydrochloride; In toluene; at 110 ℃; for 10h;

DOI:10.1021/ol4030875

Reference yield: 88.0%

→ o-nitrophenyl-N,N-dimethylcarbamate (3373-86-2)

Guidance literature:

Reference yield: 21.0%

N,N-dimethyl-formamide (68-12-2,33513-42-7) + 2-hydroxynitrobenzene (88-75-5,78813-12-4) → o-nitrophenyl-N,N-dimethylcarbamate (3373-86-2)

Guidance literature:

With tert.-butylhydroperoxide; copper(l) chloride; at 80 ℃; for 0.25h;

DOI:10.1021/jo402798k

upstream raw materials:

2-hydroxynitrobenzene

N,N-Dimethylcarbamoyl chloride

N,N-dimethyl-formamide

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