Technology Process of C30H34N6O4
There total 6 articles about C30H34N6O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
morpholine; 4-bromocrotonic acid;
With
N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
for 18h;
C22H23N5O2;
With
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
N,N-dimethyl-formamide;
for 18h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: triethylamine; dmap / dichloromethane / 24 h
2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 18 h / 70 °C
3.1: hydrogenchloride; acetic acid / water / 10 h / 90 °C
4.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 18 h
4.2: 18 h
With
hydrogenchloride; dmap; sodium hydride; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; water; N,N-dimethyl-formamide; mineral oil;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 18 h / 70 °C
2.1: hydrogenchloride; acetic acid / water / 10 h / 90 °C
3.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 18 h
3.2: 18 h
With
hydrogenchloride; sodium hydride; acetic acid; N-ethyl-N,N-diisopropylamine;
In
water; N,N-dimethyl-formamide; mineral oil;