5-(2-(4-iodophenyl)-4-(thiazol-5-yl)-1H-imidazol-1-yl)-2-methylpyridine

Base Information

Chemical Name:5-(2-(4-iodophenyl)-4-(thiazol-5-yl)-1H-imidazol-1-yl)-2-methylpyridine
CAS No.:1001014-71-6
Molecular Formula:C₁₈H₁₃IN₄S
Molecular Weight:444.299
Hs Code.:

Synonyms:5-(2-(4-iodophenyl)-4-(thiazol-5-yl)-1H-imidazol-1-yl)-2-methylpyridine

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Chemical Property of 5-(2-(4-iodophenyl)-4-(thiazol-5-yl)-1H-imidazol-1-yl)-2-methylpyridine

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Technology Process of 5-(2-(4-iodophenyl)-4-(thiazol-5-yl)-1H-imidazol-1-yl)-2-methylpyridine

There total 4 articles about 5-(2-(4-iodophenyl)-4-(thiazol-5-yl)-1H-imidazol-1-yl)-2-methylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

: 231297-35-1
2-bromo-1-(thiazol-5-yl)ethanone hydrobromide

: 1001013-84-8
(E)-4-iodo-N'-(6-methylpyridin-3-yl)benzamidine

: 1001014-71-6
5-(2-(4-iodophenyl)-4-(thiazol-5-yl)-1H-imidazol-1-yl)-2-methylpyridine

Guidance literature:: 2-bromo-1-(thiazol-5-yl)ethanone hydrobromide; (E)-4-iodo-N'-(6-methylpyridin-3-yl)benzamidine; With potassium hydrogencarbonate; In tert-butyl alcohol; at 50 ℃; for 17h;

With acetic acid; at 90 ℃; for 0.333333h;

Reference yield:

: 91516-28-8
1-(thiazol-5-yl) ethan-1-one

: 1001014-71-6
5-(2-(4-iodophenyl)-4-(thiazol-5-yl)-1H-imidazol-1-yl)-2-methylpyridine

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridinium hydrobromide perbromide; hydrogen bromide; acetic acid / 15 h / 20 °C

2.1: potassium hydrogencarbonate / tert-butyl alcohol / 17 h / 50 °C

2.2: 0.33 h / 90 °C

With pyridinium hydrobromide perbromide; hydrogen bromide; potassium hydrogencarbonate; acetic acid; In tert-butyl alcohol;

Reference yield:

: 80287-53-2,3430-14-6
5-Amino-2-methylpyridine

: 1001014-71-6
5-(2-(4-iodophenyl)-4-(thiazol-5-yl)-1H-imidazol-1-yl)-2-methylpyridine

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / dichloromethane / 18 h / 0 - 20 °C

2.1: trichlorophosphate / 18 h / 105 °C

2.2: 1.75 h / 0 - 20 °C

3.1: potassium hydrogencarbonate / tert-butyl alcohol / 17 h / 50 °C

3.2: 0.33 h / 90 °C

With potassium hydrogencarbonate; triethylamine; trichlorophosphate; In dichloromethane; tert-butyl alcohol;