C₆H₅CH₂OCOCCH₃(CH₂OCOCH₂CH₂C₂B₁₀H₁₁)2

Base Information

• Chemical Name: C₆H₅CH₂OCOCCH₃(CH₂OCOCH₂CH₂C₂B₁₀H₁₁)2
• CAS No.: 620610-55-1
• Molecular Formula: C₂₂H₄₄B₂₀O₆
• Molecular Weight: 620.808
• Mol file: 620610-55-1.mol

Synonyms:C₆H₅CH₂OCOCCH₃(CH₂OCOCH₂CH₂C₂B₁₀H₁₁)2

Chemical Property of C₆H₅CH₂OCOCCH₃(CH₂OCOCH₂CH₂C₂B₁₀H₁₁)2

Chemical Property:

Purity/Quality:

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Technology Process of C₆H₅CH₂OCOCCH₃(CH₂OCOCH₂CH₂C₂B₁₀H₁₁)2

There total 1 articles about C₆H₅CH₂OCOCCH₃(CH₂OCOCH₂CH₂C₂B₁₀H₁₁)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

3-(1',2'-dicarbo-closo-dodecaborane-1'-yl)propanoic acid (20693-22-5) + benzyl 2,2-bis(hydroxylmethyl)propionate (179388-73-9) → C6H5CH2OCOCCH3(CH2OCOCH2CH2C2B10H11)2 (620610-55-1)

Guidance literature:

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; (N2); dissolving boron compd. with dendron and EDC in CH2Cl2, addn. of DMAP, stirring for 24 h; addn. of CH2Cl2, washing org. phase with water, 10% NaHCO3, brine, drying over Na2SO4, evapn. in vac., chromy. (silica gel, hexanes to hexanes/ethyl acetate 70:30);

DOI:10.1021/ic060866r

upstream raw materials:

3-(1',2'-dicarbo-closo-dodecaborane-1'-yl)propanoic acid

benzyl 2,2-bis(hydroxylmethyl)propionate