(E)-1-(((3,7-dimethylocta-2,6-dien-1-yl)oxy)methyl)-3,5-dimethoxybenzene

Base Information

Chemical Name:(E)-1-(((3,7-dimethylocta-2,6-dien-1-yl)oxy)methyl)-3,5-dimethoxybenzene
CAS No.:1426824-94-3
Molecular Formula:C₁₉H₂₈O₃
Molecular Weight:304.43
Hs Code.:

Synonyms:(E)-1-(((3,7-dimethylocta-2,6-dien-1-yl)oxy)methyl)-3,5-dimethoxybenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-1-(((3,7-dimethylocta-2,6-dien-1-yl)oxy)methyl)-3,5-dimethoxybenzene

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Technology Process of (E)-1-(((3,7-dimethylocta-2,6-dien-1-yl)oxy)methyl)-3,5-dimethoxybenzene

There total 3 articles about (E)-1-(((3,7-dimethylocta-2,6-dien-1-yl)oxy)methyl)-3,5-dimethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 106-24-1
Geraniol

: 877-88-3
3,5-dimethoxybenzyl bromide

: 1426824-94-3
(E)-1-(((3,7-dimethylocta-2,6-dien-1-yl)oxy)methyl)-3,5-dimethoxybenzene

Guidance literature:: Geraniol; With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃; for 0.75h; Glovebox; Inert atmosphere;

3,5-dimethoxybenzyl bromide; In tetrahydrofuran; for 16h; Inert atmosphere; Reflux;
DOI:10.1002/anie.201208066

Reference yield:

: 1426824-93-2
(E)-1-(((3,7-dimethylocta-2,6-dien-1-yl)oxy)methyl)-2-methoxybenzene

: 1426824-94-3
(E)-1-(((3,7-dimethylocta-2,6-dien-1-yl)oxy)methyl)-3,5-dimethoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: N¹,N¹,N¹²,N¹²-tetramethyl-7,8-dihydro-6H-dipyrido[1,2-a:2,1'-c][1,4]diazepine-2,12-diamine / N,N-dimethyl-formamide / 72 h / Inert atmosphere; Glovebox; UV-irradiation

2.1: sodium hydride / tetrahydrofuran / 0.75 h / 0 - 20 °C / Glovebox; Inert atmosphere

2.2: 16 h / Inert atmosphere; Reflux

With N¹,N¹,N¹²,N¹²-tetramethyl-7,8-dihydro-6H-dipyrido[1,2-a:2,1'-c][1,4]diazepine-2,12-diamine; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/anie.201208066

Reference yield:

: 82529-81-5
(E)-1-(1-((3,7-dimethylocta-2,6-dien-1-yl)oxy)methyl)-4-methoxybenzene

: 1426824-94-3
(E)-1-(((3,7-dimethylocta-2,6-dien-1-yl)oxy)methyl)-3,5-dimethoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: N¹,N¹,N¹²,N¹²-tetramethyl-7,8-dihydro-6H-dipyrido[1,2-a:2,1'-c][1,4]diazepine-2,12-diamine / N,N-dimethyl-formamide / 72 h / Inert atmosphere; Glovebox; UV-irradiation

2.1: sodium hydride / tetrahydrofuran / 0.75 h / 0 - 20 °C / Glovebox; Inert atmosphere

2.2: 16 h / Inert atmosphere; Reflux

With N¹,N¹,N¹²,N¹²-tetramethyl-7,8-dihydro-6H-dipyrido[1,2-a:2,1'-c][1,4]diazepine-2,12-diamine; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/anie.201208066