potassium 1-(3-(tert-butyl)-5-(1-methylcyclopropyl)phenyl)-5-(cyclohexyloxy)-1H-pyrazole-3-carboxylate

Base Information

Chemical Name:potassium 1-(3-(tert-butyl)-5-(1-methylcyclopropyl)phenyl)-5-(cyclohexyloxy)-1H-pyrazole-3-carboxylate
CAS No.:1561965-88-5
Molecular Formula:C₂₄H₃₁N₂O₃*K
Molecular Weight:434.62
Hs Code.:

Synonyms:potassium 1-(3-(tert-butyl)-5-(1-methylcyclopropyl)phenyl)-5-(cyclohexyloxy)-1H-pyrazole-3-carboxylate

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Chemical Property of potassium 1-(3-(tert-butyl)-5-(1-methylcyclopropyl)phenyl)-5-(cyclohexyloxy)-1H-pyrazole-3-carboxylate

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Technology Process of potassium 1-(3-(tert-butyl)-5-(1-methylcyclopropyl)phenyl)-5-(cyclohexyloxy)-1H-pyrazole-3-carboxylate

There total 7 articles about potassium 1-(3-(tert-butyl)-5-(1-methylcyclopropyl)phenyl)-5-(cyclohexyloxy)-1H-pyrazole-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1561965-85-2
ethyl 1-(3-(tert-butyl)-5-(1-methylcyclopropyl)phenyl)-5-(cyclohexyloxy)-1H-pyrazole-3-carboxylate

: 1561965-88-5
potassium 1-(3-(tert-butyl)-5-(1-methylcyclopropyl)phenyl)-5-(cyclohexyloxy)-1H-pyrazole-3-carboxylate

Guidance literature:: With potassium hydroxide; In methanol;

Reference yield:

: 129316-09-2
1,3-dibromo-5-t-butylbenzene

: 1561965-88-5
potassium 1-(3-(tert-butyl)-5-(1-methylcyclopropyl)phenyl)-5-(cyclohexyloxy)-1H-pyrazole-3-carboxylate

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; 1,4-dioxane / 90 °C / Inert atmosphere

2.1: trifluoroacetic acid; diethylzinc / hexane; dichloromethane / 0 °C

2.2: 0.5 h / 0 - 20 °C

3.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,4-dioxane / 16 h / 100 °C / Inert atmosphere

4.1: copper diacetate; pyridine / N,N-dimethyl-formamide / 36 h / 40 °C / Inert atmosphere

5.1: potassium hydroxide / methanol

With pyridine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; diethylzinc; potassium acetate; copper diacetate; potassium carbonate; trifluoroacetic acid; potassium hydroxide; In 1,4-dioxane; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 1403387-36-9
1-bromo-3-(tert-butyl)-5-(prop-1-en-2-yl)benzene

: 1561965-88-5
potassium 1-(3-(tert-butyl)-5-(1-methylcyclopropyl)phenyl)-5-(cyclohexyloxy)-1H-pyrazole-3-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1.1: trifluoroacetic acid; diethylzinc / hexane; dichloromethane / 0 °C

1.2: 0.5 h / 0 - 20 °C

2.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,4-dioxane / 16 h / 100 °C / Inert atmosphere

3.1: copper diacetate; pyridine / N,N-dimethyl-formamide / 36 h / 40 °C / Inert atmosphere

4.1: potassium hydroxide / methanol

With pyridine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; diethylzinc; potassium acetate; copper diacetate; trifluoroacetic acid; potassium hydroxide; In 1,4-dioxane; methanol; hexane; dichloromethane; N,N-dimethyl-formamide;