O-(1-benzylindolin-5-yl)-N-methyl-N-(4-tetrahydropyranylmethyl)carbamate

Base Information

Chemical Name:O-(1-benzylindolin-5-yl)-N-methyl-N-(4-tetrahydropyranylmethyl)carbamate
CAS No.:1239325-19-9
Molecular Formula:C₂₃H₂₈N₂O₃
Molecular Weight:380.487
Hs Code.:

Synonyms:O-(1-benzylindolin-5-yl)-N-methyl-N-(4-tetrahydropyranylmethyl)carbamate

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Chemical Property of O-(1-benzylindolin-5-yl)-N-methyl-N-(4-tetrahydropyranylmethyl)carbamate

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Technology Process of O-(1-benzylindolin-5-yl)-N-methyl-N-(4-tetrahydropyranylmethyl)carbamate

There total 4 articles about O-(1-benzylindolin-5-yl)-N-methyl-N-(4-tetrahydropyranylmethyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: N-methyl-N-(tetrahydro-pyran-4-ylmethyl) amine hydrochloride

: 1239325-57-5
1-benzylindolin-5-yl-4-nitrophenylcarbonate

: 1239325-19-9
O-(1-benzylindolin-5-yl)-N-methyl-N-(4-tetrahydropyranylmethyl)carbamate

Guidance literature:: With triethylamine; In acetonitrile; for 1h; Cooling with ice;

Reference yield:

: 666262-72-2
N-(tetrahydro-pyran-4-ylmethyl)-carbamic acid tert-butyl ester

: 1239325-19-9
O-(1-benzylindolin-5-yl)-N-methyl-N-(4-tetrahydropyranylmethyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 20 °C / Cooling with ice

2: hydrogenchloride / ethyl acetate / 1.5 h / 20 °C

3: triethylamine / acetonitrile / 1 h / Cooling with ice

With hydrogenchloride; sodium hydride; triethylamine; In ethyl acetate; N,N-dimethyl-formamide; acetonitrile; mineral oil;

Reference yield:

: 666262-73-3
N-methyl-N-(tetrahydro-pyran-4-ylmethyl)-carbamic acid tert-butyl ester

: 1239325-19-9
O-(1-benzylindolin-5-yl)-N-methyl-N-(4-tetrahydropyranylmethyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / ethyl acetate / 1.5 h / 20 °C

2: triethylamine / acetonitrile / 1 h / Cooling with ice

With hydrogenchloride; triethylamine; In ethyl acetate; acetonitrile;