methyl (4S)-2-(2-allyloxy-3-bromophenyl)-5-benzyloxy-3-oxo-4-[N-(Boc)amino]pentanoate

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Chemical Name:methyl (4S)-2-(2-allyloxy-3-bromophenyl)-5-benzyloxy-3-oxo-4-[N-(Boc)amino]pentanoate
CAS No.:1057669-18-7
Molecular Formula:C₂₇H₃₂BrNO₇
Molecular Weight:562.458
Hs Code.:

Synonyms:methyl (4S)-2-(2-allyloxy-3-bromophenyl)-5-benzyloxy-3-oxo-4-[N-(Boc)amino]pentanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (4S)-2-(2-allyloxy-3-bromophenyl)-5-benzyloxy-3-oxo-4-[N-(Boc)amino]pentanoate

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Technology Process of methyl (4S)-2-(2-allyloxy-3-bromophenyl)-5-benzyloxy-3-oxo-4-[N-(Boc)amino]pentanoate

There total 1 articles about methyl (4S)-2-(2-allyloxy-3-bromophenyl)-5-benzyloxy-3-oxo-4-[N-(Boc)amino]pentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1057669-17-6
C₁₂H₁₃BrO₃

: 23680-31-1
BOC-O-benzyl-L-serine

: 1057669-18-7
methyl (4S)-2-(2-allyloxy-3-bromophenyl)-5-benzyloxy-3-oxo-4-[N-(Boc)amino]pentanoate

Guidance literature:: BOC-O-benzyl-L-serine; With 1,1'-carbonyldiimidazole; In tetrahydrofuran; for 2h; Inert atmosphere;

C₁₂H₁₃BrO₃; With lithium diisopropyl amide; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol8014336

Reference yield: 80.0%

: 1057669-18-7
methyl (4S)-2-(2-allyloxy-3-bromophenyl)-5-benzyloxy-3-oxo-4-[N-(Boc)amino]pentanoate

: 1057669-20-1
C₂₄H₂₈BrNO₇

Guidance literature:: With trans-bis(triphenylphosphine)palladium dichloride; tri-n-butyl-tin hydride; In tetrahydrofuran;
DOI:10.1021/ol8014336