o-phenyl hexylcarbamothioate

Base Information

• Chemical Name: o-phenyl hexylcarbamothioate
• CAS No.: 1436862-82-6
• Molecular Formula: C₁₃H₁₉NOS
• Molecular Weight: 237.366

Synonyms:o-phenyl hexylcarbamothioate

Chemical Property of o-phenyl hexylcarbamothioate

Chemical Property:

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MSDS Files:

SDS file from LookChem

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Technology Process of o-phenyl hexylcarbamothioate

There total 1 articles about o-phenyl hexylcarbamothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

hexan-1-amine (111-26-2) + phenylcarbonochloridothioate (1005-56-7) → o-phenyl hexylcarbamothioate (1436862-82-6)

Guidance literature:

In dichloromethane; at 20 ℃; for 0.5h;

DOI:10.1055/s-0033-1338744

Reference yield: 98.0%

o-phenyl hexylcarbamothioate (1436862-82-6) → n-hexyl isothiocyanate (4404-45-9)

Guidance literature:

With sodium hydroxide; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1055/s-0033-1338744

Reference yield: 97.0%

o-phenyl hexylcarbamothioate (1436862-82-6) + cyclohexylamine (108-91-8,157973-60-9) → C13H26N2S (401640-79-7)

Guidance literature:

In water; at 100 ℃; for 0.333333h; Green chemistry;

DOI:10.3184/174751916X14760947474916

upstream raw materials:

hexan-1-amine

phenylcarbonochloridothioate

Downstream raw materials:

n-hexyl isothiocyanate

C₁₃H₂₆N₂S

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