C₂₇H₂₉N₃O₇

Base Information

Chemical Name:C₂₇H₂₉N₃O₇
CAS No.:1315455-49-2
Molecular Formula:C₂₇H₂₉N₃O₇
Molecular Weight:507.543
Hs Code.:

C<sub>27</sub>H<sub>29</sub>N<sub>3</sub>O<sub>7</sub>

Synonyms:C₂₇H₂₉N₃O₇

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Chemical Property of C₂₇H₂₉N₃O₇

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Technology Process of C₂₇H₂₉N₃O₇

There total 22 articles about C₂₇H₂₉N₃O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: C₂₇H₃₁N₃O₇

: 1315455-49-2
C₂₇H₂₉N₃O₇

Guidance literature:: With bis{rhodium[3,3'-(1,3-phenylene)bis(2,2-dimethylpropanoic acid)]}; PhI(OPiv)2; magnesium oxide; In 1,2-dichloro-ethane; at 20 - 60 ℃; Inert atmosphere;
DOI:10.1002/chem.201003489

Reference yield:

: 885703-19-5
(3S,4S)-4-N-phthalimido-1,5-hexadiene-3-ol

: 1315455-49-2
C₂₇H₂₉N₃O₇

Guidance literature:: Multi-step reaction with 18 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 11 h / 20 °C / Inert atmosphere

2.1: osmium(VIII) oxide; (8a,9R,8′′′a,9′′′R)-9,9′-[(2,5-diphenylpyrimidine-4,6-diyl)bis(oxy)]bis(6′-methoxy-10,11-dihydrocinchonan); methanesulfonamide; sodium hydrogencarbonate; potassium carbonate; potassium hexacyanoferrate(III) / water; tert-butyl alcohol / 6 h / 5 °C / Inert atmosphere

3.1: nitrogen; methylamine / water / 1 h / 50 °C / 10 Torr / Inert atmosphere

4.1: sodium hydrogencarbonate / ethyl acetate / 1.5 h / Inert atmosphere

5.1: dmap; triethylamine; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.03 h / 0 - 20 °C / Inert atmosphere

6.1: dichloromethane / 1 h / -40 °C / Inert atmosphere

7.1: caesium carbonate / N,N-dimethyl-formamide / 4 h / 60 °C / Inert atmosphere

8.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 2 h / Inert atmosphere

9.1: Dess-Martin periodane / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

10.1: acetic acid / chloroform / 12 h / 20 °C / Molecular sieve; Inert atmosphere

11.1: sodium cyanoborohydride / tetrahydrofuran / 2 h / Inert atmosphere

12.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

13.1: dmap; potassium carbonate / dichloromethane / 20 °C / Inert atmosphere

14.1: 1,4-diaza-bicyclo[2.2.2]octane; bis(1,5-cyclooctadiene)diiridium(I) dichloride; (3,5-dioxa-4-phospha-cyclohepta[2,1-a;3,4-a']dinaphthalen-4-yl)-bis-(1-phenyl-ethyl)-amine / tetrahydrofuran / 20 °C / Inert atmosphere

15.1: palladium diacetate; silver nitrate; triphenylphosphine / 1,4-dioxane / 1 h / 80 °C / Inert atmosphere

16.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 20 °C / Inert atmosphere

16.2: 2 h / aq. phosphate buffer

17.1: dichloromethane / 1 h / 0 °C / Inert atmosphere

18.1: bis{rhodium[3,3'-(1,3-phenylene)bis(2,2-dimethylpropanoic acid)]}; PhI(OPiv)2; magnesium oxide / 1,2-dichloro-ethane / 20 - 60 °C / Inert atmosphere

With 1,4-diaza-bicyclo[2.2.2]octane; 1H-imidazole; dmap; osmium(VIII) oxide; bis(1,5-cyclooctadiene)diiridium(I) dichloride; (8a,9R,8′′′a,9′′′R)-9,9′-[(2,5-diphenylpyrimidine-4,6-diyl)bis(oxy)]bis(6′-methoxy-10,11-dihydrocinchonan); methanesulfonamide; bis{rhodium[3,3'-(1,3-phenylene)bis(2,2-dimethylpropanoic acid)]}; PhI(OPiv)2; nitrogen; tetrabutyl ammonium fluoride; palladium diacetate; magnesium oxide; sodium cyanoborohydride; sodium hydrogencarbonate; potassium carbonate; caesium carbonate; Dess-Martin periodane; silver nitrate; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; 9-bora-bicyclo[3.3.1]nonane; triphenylphosphine; methylamine; (3,5-dioxa-4-phospha-cyclohepta[2,1-a;3,4-a']dinaphthalen-4-yl)-bis-(1-phenyl-ethyl)-amine; potassium hexacyanoferrate(III); In tetrahydrofuran; 1,4-dioxane; dichloromethane; chloroform; water; ethyl acetate; 1,2-dichloro-ethane; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1002/chem.201003489

Reference yield:

: 1016976-14-9
methyl 3-amino-5-benzyloxy-4-iodobenzoate

: 1315455-49-2
C₂₇H₂₉N₃O₇

Guidance literature:: Multi-step reaction with 9 steps

1.1: acetic acid / chloroform / 12 h / 20 °C / Molecular sieve; Inert atmosphere

2.1: sodium cyanoborohydride / tetrahydrofuran / 2 h / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

4.1: dmap; potassium carbonate / dichloromethane / 20 °C / Inert atmosphere

5.1: 1,4-diaza-bicyclo[2.2.2]octane; bis(1,5-cyclooctadiene)diiridium(I) dichloride; (3,5-dioxa-4-phospha-cyclohepta[2,1-a;3,4-a']dinaphthalen-4-yl)-bis-(1-phenyl-ethyl)-amine / tetrahydrofuran / 20 °C / Inert atmosphere

6.1: palladium diacetate; silver nitrate; triphenylphosphine / 1,4-dioxane / 1 h / 80 °C / Inert atmosphere

7.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 20 °C / Inert atmosphere

7.2: 2 h / aq. phosphate buffer

8.1: dichloromethane / 1 h / 0 °C / Inert atmosphere

9.1: bis{rhodium[3,3'-(1,3-phenylene)bis(2,2-dimethylpropanoic acid)]}; PhI(OPiv)2; magnesium oxide / 1,2-dichloro-ethane / 20 - 60 °C / Inert atmosphere

With 1,4-diaza-bicyclo[2.2.2]octane; dmap; bis(1,5-cyclooctadiene)diiridium(I) dichloride; bis{rhodium[3,3'-(1,3-phenylene)bis(2,2-dimethylpropanoic acid)]}; PhI(OPiv)2; tetrabutyl ammonium fluoride; palladium diacetate; magnesium oxide; sodium cyanoborohydride; potassium carbonate; silver nitrate; acetic acid; 9-bora-bicyclo[3.3.1]nonane; triphenylphosphine; (3,5-dioxa-4-phospha-cyclohepta[2,1-a;3,4-a']dinaphthalen-4-yl)-bis-(1-phenyl-ethyl)-amine; In tetrahydrofuran; 1,4-dioxane; dichloromethane; chloroform; 1,2-dichloro-ethane;
DOI:10.1002/chem.201003489