chloro[2-(phenyldiazenyl-κN2)pyridine-κN](2,2':6',2''-terpyridine-κ3N)ruthenium(II) chloride

Base Information

Chemical Name:chloro[2-(phenyldiazenyl-κN2)pyridine-κN](2,2':6',2''-terpyridine-κ3N)ruthenium(II) chloride
CAS No.:173343-62-9
Molecular Formula:C₂₆H₂₀ClN₆Ru*Cl
Molecular Weight:588.461
Hs Code.:

Synonyms:chloro[2-(phenyldiazenyl-κN2)pyridine-κN](2,2':6',2''-terpyridine-κ3N)ruthenium(II) chloride

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Chemical Property of chloro[2-(phenyldiazenyl-κN2)pyridine-κN](2,2':6',2''-terpyridine-κ3N)ruthenium(II) chloride

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Technology Process of chloro[2-(phenyldiazenyl-κN2)pyridine-κN](2,2':6',2''-terpyridine-κ3N)ruthenium(II) chloride

There total 1 articles about chloro[2-(phenyldiazenyl-κN2)pyridine-κN](2,2':6',2''-terpyridine-κ3N)ruthenium(II) chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 2569-57-5
2-(phenylazo)pyridine

: 72905-30-7
(2,2':6',2''-terpyridine)trichlororuthenium(III)

: 173343-62-9
chloro[2-(phenyldiazenyl-κN2)pyridine-κN](2,2':6',2''-terpyridine-κ3N)ruthenium(II) chloride

Guidance literature:: With triethylamine; LiCl; In ethanol; water; amine addn. to educts and LiCl soln., reflux (4 h); cooling, filtration, volume reduction (reduced pressure), standing (overnight, 4°C), ppt. filtration, recrystallization (boiling water); elem. anal.;
DOI:10.1016/1381-1169(95)00112-3

Reference yield: 43.0%

: 173343-62-9
chloro[2-(phenyldiazenyl-κN2)pyridine-κN](2,2':6',2''-terpyridine-κ3N)ruthenium(II) chloride

: silver perchlorate

: (2,2':6',2''-terpyridine)(2-phenylazopyridine)(aquo)ruthenium(II) perchlorate

Guidance literature:: With NaClO₄; In water; acetone; dissolving, reflux (1.5 h); filtration, volume reduction (reduced pressure), NaClO4 saturated soln. addn.; elem. anal.;
DOI:10.1016/1381-1169(95)00112-3

Reference yield: 15.0%

: 17084-13-8
potassium hexafluorophosphate

: 173343-62-9
chloro[2-(phenyldiazenyl-κN2)pyridine-κN](2,2':6',2''-terpyridine-κ3N)ruthenium(II) chloride

: 1244959-03-2
2-[2-(2-thioacetyl)ethoxy]ethyl 2,3,4,6-tetraacetate-β-D-glucopyranoside

: C₃₉H₄₆N₆O₈RuS⁽²⁺⁾*F₆P^(2-)

Guidance literature:: chloro[2-(phenyldiazenyl-κN2)pyridine-κN](2,2':6',2''-terpyridine-κ3N)ruthenium(II) chloride; 2-[2-(2-thioacetyl)ethoxy]ethyl 2,3,4,6-tetraacetate-β-D-glucopyranoside; In water; at 80 ℃; Inert atmosphere; Darkness;

potassium hexafluorophosphate; Inert atmosphere;
DOI:10.1002/chem.201705388