methyl 3-amino-2-butyramidobenzoate

Base Information

• Chemical Name: methyl 3-amino-2-butyramidobenzoate
• CAS No.: 1207547-73-6
• Molecular Formula: C₁₂H₁₆N₂O₃
• Molecular Weight: 236.271
• Mol file: 1207547-73-6.mol

Synonyms:methyl 3-amino-2-butyramidobenzoate

Chemical Property of methyl 3-amino-2-butyramidobenzoate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of methyl 3-amino-2-butyramidobenzoate

There total 5 articles about methyl 3-amino-2-butyramidobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

methyl 2-butylamido-3-nitrobenzoate (136285-39-7) → methyl 3-amino-2-butyramidobenzoate (1207547-73-6)

Guidance literature:

With hydrogen; palladium 10% on activated carbon; In methanol; at 20 ℃; for 6h;

Reference yield:

C12H13BrN2O5 → methyl 3-amino-2-butyramidobenzoate (1207547-73-6)

Guidance literature:

With hydrogen; palladium 10% on activated carbon; In methanol; at 20 ℃; for 7h;

Reference yield:

methyl 2-butyrylaminobenzoate (30006-30-5) → methyl 3-amino-2-butyramidobenzoate (1207547-73-6)

Guidance literature:

Multi-step reaction with 2 steps

1: nitric acid / 0.33 h / 0 °C

2: hydrogen / palladium 10% on activated carbon / methanol / 6 h / 20 °C

With hydrogen; nitric acid; palladium 10% on activated carbon; In methanol;

upstream raw materials:

2-carbomethoxyaniline

methyl 2-butylamido-3-nitrobenzoate

5-bromo-2-aminobenzoic acid methyl ester

methyl 2-butyrylaminobenzoate

Refernces