6,7,9,10,12,13,15,16-Octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecene-2-carboxylic acid 4'-cyano-biphenyl-4-yl ester

Base Information

Chemical Name:6,7,9,10,12,13,15,16-Octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecene-2-carboxylic acid 4'-cyano-biphenyl-4-yl ester
CAS No.:113398-39-3
Molecular Formula:C₂₈H₂₇NO₇
Molecular Weight:489.525
Hs Code.:

Synonyms:6,7,9,10,12,13,15,16-Octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecene-2-carboxylic acid 4'-cyano-biphenyl-4-yl ester

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Chemical Property of 6,7,9,10,12,13,15,16-Octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecene-2-carboxylic acid 4'-cyano-biphenyl-4-yl ester

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Technology Process of 6,7,9,10,12,13,15,16-Octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecene-2-carboxylic acid 4'-cyano-biphenyl-4-yl ester

There total 2 articles about 6,7,9,10,12,13,15,16-Octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecene-2-carboxylic acid 4'-cyano-biphenyl-4-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 19812-93-2
4-Cyano-4'-hydroxybiphenyl

: 54664-43-6
4'-benzo-15-crown-5-carboxylic acid chloride

: 113398-39-3
6,7,9,10,12,13,15,16-Octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecene-2-carboxylic acid 4'-cyano-biphenyl-4-yl ester

Guidance literature:: With pyridine; In benzene; for 5h; Heating;
DOI:10.1021/jo00289a028

Reference yield:

: 56683-55-7
2,3-(4'-carboxybenzo)-1,4,7,10,13-pentaoxacyclopentadeca-2-ene

: 113398-39-3
6,7,9,10,12,13,15,16-Octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecene-2-carboxylic acid 4'-cyano-biphenyl-4-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / Heating

2: 70 percent / pyridine / benzene / 5 h / Heating

With pyridine; thionyl chloride; In benzene;
DOI:10.1021/jo00289a028