N,N-(2-methoxy-5-nitro-1,3-phenylene)bisurea>

Base Information

Chemical Name:N,N-(2-methoxy-5-nitro-1,3-phenylene)bisurea>
CAS No.:140362-03-4
Molecular Formula:C₂₉H₃₅N₅O₉
Molecular Weight:597.625
Hs Code.:

N,N-(2-methoxy-5-nitro-1,3-phenylene)bis<N'-<2-methoxy-3-(methoxymethyl)-5-methylphenyl>urea>

Synonyms:N,N-(2-methoxy-5-nitro-1,3-phenylene)bisurea>

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Chemical Property of N,N-(2-methoxy-5-nitro-1,3-phenylene)bisurea>

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Technology Process of N,N-(2-methoxy-5-nitro-1,3-phenylene)bisurea>

There total 1 articles about N,N-(2-methoxy-5-nitro-1,3-phenylene)bisurea> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 129125-24-2
2-methoxy-3-(methoxymethyl)-5-methylbenzeneamine

: 1,3-Diisocyanato-2-methoxy-5-nitro-benzene

: 140362-03-4
N,N-(2-methoxy-5-nitro-1,3-phenylene)bisurea>

Guidance literature:: In toluene; Yield given; 1.) 90 deg C, 3 h, 2.) r.t., overnight;
DOI:10.1021/jo00036a009

Reference yield: 48.0%

: 5469-66-9
propane-1,3-diol ditosylate

: 140362-03-4
N,N-(2-methoxy-5-nitro-1,3-phenylene)bisurea>

: 140362-04-5
1,1'-(2-methoxy-5-nitro-1,3-phenylene)bis-2(1H)-pyrimidinone>

Guidance literature:: With sodium hydroxide; trimethylbenzylammonium bromide; In water; benzene; for 168h; Ambient temperature;
DOI:10.1021/jo00036a009

Reference yield:

: 140362-03-4
N,N-(2-methoxy-5-nitro-1,3-phenylene)bisurea>

: C₃₉H₄₀N₈O₁₁S*BrNa

Guidance literature:: Multi-step reaction with 5 steps

1: 48 percent / NaOH / benzyltrimethylammonium bromide / H₂O; benzene / 168 h / Ambient temperature

2: 55 percent / Fe(CO)5, 1N NaOH / benzene / 18 h / Ambient temperature

3: 82 percent / NaHCO₃ / methanol / 72 h

4: 91 percent / HBr gas / CHCl₃ / 0.75 h

5: 41 percent / Na₂S*9H₂O / ethanol; benzene / 12 h

With sodium sulfide; sodium hydroxide; iron pentacarbonyl; hydrogen bromide; sodium hydrogencarbonate; trimethylbenzylammonium bromide; In methanol; ethanol; chloroform; water; benzene;
DOI:10.1021/jo00036a009