ethyl hydrogen benzyloxymethylphosphonate

Base Information

Chemical Name:ethyl hydrogen benzyloxymethylphosphonate
CAS No.:240432-39-7
Molecular Formula:C₁₀H₁₅O₄P
Molecular Weight:230.2
Hs Code.:

Synonyms:ethyl hydrogen benzyloxymethylphosphonate

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Chemical Property of ethyl hydrogen benzyloxymethylphosphonate

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Technology Process of ethyl hydrogen benzyloxymethylphosphonate

There total 1 articles about ethyl hydrogen benzyloxymethylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 89268-01-9
(phenylmethoxy)methylphosphonic acid diethyl ester

: 240432-39-7
ethyl hydrogen benzyloxymethylphosphonate

Guidance literature:: With potassium hydroxide; In ethanol; at 75 ℃; for 2.5h;
DOI:10.1021/jm991008q

Reference yield:

: 240432-39-7
ethyl hydrogen benzyloxymethylphosphonate

: 240432-40-0
ethyl benzyloxymethyl(chloro)phosphonate

Guidance literature:: With oxalyl dichloride; N,N-dimethyl-formamide; In benzene; for 2.5h; Ambient temperature;
DOI:10.1021/jm991008q

Reference yield:

: 240432-39-7
ethyl hydrogen benzyloxymethylphosphonate

: 240432-41-1
ethyl benzyloxymethyl<(diethoxyphosphoryl)methyl>phosphinate

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl chloride, DMF / benzene / 2.5 h / Ambient temperature

2: 1.) n-butyllithium / 1.) cyclohexane, THF, -78 deg C, 15 min, 2.) cyclohexane, THF, a) -78 deg C, 1 h, b) 0 deg C, 1 h

With n-butyllithium; oxalyl dichloride; N,N-dimethyl-formamide; In benzene;
DOI:10.1021/jm991008q