[(4aS,8aS)-3,4,4a,5,6,7,8,8a-octahydro-2,5,5,8a-tetramethylnaphthalen-1-yl]acetaldehyde

Base Information

Chemical Name:[(4aS,8aS)-3,4,4a,5,6,7,8,8a-octahydro-2,5,5,8a-tetramethylnaphthalen-1-yl]acetaldehyde
CAS No.:68985-11-5
Molecular Formula:C₁₆H₂₆O
Molecular Weight:234.382
Hs Code.:

Synonyms:[(4aS,8aS)-3,4,4a,5,6,7,8,8a-octahydro-2,5,5,8a-tetramethylnaphthalen-1-yl]acetaldehyde

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Chemical Property of [(4aS,8aS)-3,4,4a,5,6,7,8,8a-octahydro-2,5,5,8a-tetramethylnaphthalen-1-yl]acetaldehyde

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of [(4aS,8aS)-3,4,4a,5,6,7,8,8a-octahydro-2,5,5,8a-tetramethylnaphthalen-1-yl]acetaldehyde

There total 12 articles about [(4aS,8aS)-3,4,4a,5,6,7,8,8a-octahydro-2,5,5,8a-tetramethylnaphthalen-1-yl]acetaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 31222-15-8
2-[(4aS,8aS)-3,4,4a,5,6,7,8,8a-octahydro-2,5,5,8a-tetramethylnaphthalen-1-yl]ethanol

: 68985-11-5,97806-23-0
[(4aS,8aS)-3,4,4a,5,6,7,8,8a-octahydro-2,5,5,8a-tetramethylnaphthalen-1-yl]acetaldehyde

Guidance literature:: 2-[(4aS,8aS)-3,4,4a,5,6,7,8,8a-octahydro-2,5,5,8a-tetramethylnaphthalen-1-yl]ethanol; With phosphorus pentoxide; dimethyl sulfoxide; In dichloromethane; at 20 ℃; for 0.916667h; Cooling with ice;

With triethylamine; at 20 ℃; for 0.916667h; Cooling with ice;
DOI:10.1007/s10600-016-1854-6

Reference yield: 94.0%

: (4aR,6R,8aS)-5-[(E)-2-chloroethenyl]decahydro-1,1,4a,6-tetramethylnaphthalene

: 68985-11-5,97806-23-0
[(4aS,8aS)-3,4,4a,5,6,7,8,8a-octahydro-2,5,5,8a-tetramethylnaphthalen-1-yl]acetaldehyde

Guidance literature:: With potassium tert-butylate; In tert-butyl alcohol; at 82 ℃; for 4h;
DOI:10.1002/hlca.201300286

Reference yield: 85.0%

: 97974-42-0
1-ethynyl-2,5,5,8a-tetramethyl-perhydro-4aH-1-naphthalenol

: 68985-11-5,97806-23-0
[(4aS,8aS)-3,4,4a,5,6,7,8,8a-octahydro-2,5,5,8a-tetramethylnaphthalen-1-yl]acetaldehyde

Guidance literature:: tris-(triphenylsiloxy)-vanadium oxide; stearic acid; triphenylhydroxysilane; In o-xylene; at 145 ℃; for 7.33333h; Heating / reflux;