Technology Process of benzyl 2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside
There total 6 articles about benzyl 2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylsilane; boron trifluoride diethyl etherate;
In
dichloromethane;
at 0 ℃;
regioselective reaction;
DOI:10.1039/d1sc03188k
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C
2: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / 0 °C
With
triethylsilane; boron trifluoride diethyl etherate; sodium hydride;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/d1sc03188k
- Guidance literature:
-
Multi-step reaction with 5 steps
1: triflic azide; potassium carbonate; copper(II) sulfate / dichloromethane; water / 0 - 20 °C
2: camphor-10-sulfonic acid / acetonitrile
3: silver carbonate / acetonitrile / 60 °C
4: sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C
5: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / 0 °C
With
triethylsilane; triflic azide; camphor-10-sulfonic acid; boron trifluoride diethyl etherate; sodium hydride; potassium carbonate; copper(II) sulfate; silver carbonate;
In
dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/d1sc03188k
